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Direct polymerization of levulinic acid via Ugi multicomponent reaction
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Hartweg, Manuel and Becer, C. Remzi (2016) Direct polymerization of levulinic acid via Ugi multicomponent reaction. Green Chemistry, 18 (11). pp. 3272-3277. doi:10.1039/C6GC00372A ISSN 1463-9262.
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Official URL: http://dx.doi.org/10.1039/C6GC00372A
Abstract
A robust, direct and efficient approach has been developed for the utilization of levulinic acid (LevA) as a building block in the synthesis of polyamides. In this approach, there is no need for converting LevA to a cyclic monomer as the carboxylic acid and ketone groups are sufficient for incorporation into a polyamide. Optimization of reaction temperature, solvent, reactants as well as heating source have been performed for the Ugi multicomponent reaction. The obtained polyamides were characterized carefully using GPC, NMR, MALDI-ToF MS, DSC and TGA.
Item Type: | Journal Article | ||||||
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Divisions: | Faculty of Science, Engineering and Medicine > Science > Chemistry | ||||||
Journal or Publication Title: | Green Chemistry | ||||||
Publisher: | Royal Society of Chemistry | ||||||
ISSN: | 1463-9262 | ||||||
Official Date: | 7 June 2016 | ||||||
Dates: |
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Volume: | 18 | ||||||
Number: | 11 | ||||||
Page Range: | pp. 3272-3277 | ||||||
DOI: | 10.1039/C6GC00372A | ||||||
Status: | Peer Reviewed | ||||||
Publication Status: | Published | ||||||
Access rights to Published version: | Restricted or Subscription Access |
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