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Data for A suite of solid-state NMR experiments to utilize orphaned magnetization for assignment of proteins using parallel high and low gamma detection

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Gallo, Angelo, Franks, W. Trent and Lewandowski, Józef R. (2019) Data for A suite of solid-state NMR experiments to utilize orphaned magnetization for assignment of proteins using parallel high and low gamma detection. [Dataset]

[img] Archive (ZIP) (NMR Data for Multiple receivers)
GalFraLewJMR2019data.tar - Submitted Version
Available under License Creative Commons Attribution 4.0.

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Abstract

We present a suite of two-receiver solid-state NMR experiments for backbone and side chain resonance assignment. The experiments rely on either dipolar coupling or scalar coupling for polarization transfer and are devised to acquire a 1H–detected 3D experiment AND a nested 13C–detected 2D from a shared excitation pulse. In order to compensate for the lower sensitivity of detection on 13C nucleus, 2D rows are signal averaged during 3D planes. The 3D dual receiver experiments do not suffer from any appreciable signal loss compared to their single receiver versions and require no extra optimization. The resulting data is higher in information content with no additional experiment time. The approach is expected to become widespread as multiple receivers become standard for new NMR spectrometers.

Item Type: Dataset
Subjects: Q Science > QC Physics
Q Science > QD Chemistry
Divisions: Faculty of Science > Chemistry
Faculty of Science > Physics
Type of Data: Nuclear Magnetic Resonance - raw spectra data
Library of Congress Subject Headings (LCSH): Nuclear magnetic resonance spectroscopy, Proteins
Publisher: Chemistry, University of Warwick
Official Date: 23 July 2019
Dates:
DateEvent
3 July 2019Available
23 July 2019Published
Collection date:
Date fromDate to
1 January 201822 December 2018
Status: Not Peer Reviewed
Publication Status: Published
Media of Output: .tar
Access rights to Published version: Open Access
Copyright Holders: University of Warwick
Description:

TAR file of raw spectra data

RIOXX Funder/Project Grant:
Project/Grant IDRIOXX Funder NameFunder ID
FP/2007-2013[ERC] Horizon 2020 Framework Programmehttp://dx.doi.org/10.13039/100010661
639907[ERC] Horizon 2020 Framework Programmehttp://dx.doi.org/10.13039/100010661
BB/L022761/1[BBSRC] Biotechnology and Biological Sciences Research Councilhttp://dx.doi.org/10.13039/501100000268
BB/R010218/1[BBSRC] Biotechnology and Biological Sciences Research Councilhttp://dx.doi.org/10.13039/501100000268
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Contributors:
ContributionNameContributor ID
DistributorFranks, W. TrentUNSPECIFIED

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