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Synthesis, characterisation and molecular structure of a calcium stannyl derivative [Ca{Sn(mu-OSiMe2But)(3)}(2)]
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UNSPECIFIED (2000) Synthesis, characterisation and molecular structure of a calcium stannyl derivative [Ca{Sn(mu-OSiMe2But)(3)}(2)]. MAIN GROUP METAL CHEMISTRY, 23 (8). pp. 395-400. ISSN 0334-7575
Full text not available from this repository.Abstract
The compound, [Ca{Sn(mu-OSiMe2But)(3)}(2)] 1, was prepared by the condensation reaction of Ca(OSiMe2But)(2) with Sn(OSiMe2But)(2) in dme. The structural characterisation revealed that 1 crystallises in the monoclinic system {Space group P2(1)/n (non-standard N-o 14)}. Each of the two Sn(mu-OSiMe2But)(3) anion binds the Ca(II) cation in an eta(6) fashion [av. Ca - O 2.408 Angstrom ]. Multinuclear [C-13, Si-29 and Sn-119 ] solid-state NMR spectroscopic studies are also reported. Compound 1 showed satisfactory elemental analysis.
| Item Type: | Journal Article |
|---|---|
| Subjects: | Q Science > QD Chemistry |
| Journal or Publication Title: | MAIN GROUP METAL CHEMISTRY |
| Publisher: | FREUND PUBLISHING HOUSE LTD |
| ISSN: | 0334-7575 |
| Date: | 2000 |
| Volume: | 23 |
| Number: | 8 |
| Number of Pages: | 6 |
| Page Range: | pp. 395-400 |
| Publication Status: | Published |
| URI: | http://wrap.warwick.ac.uk/id/eprint/13109 |
Data sourced from Thomson Reuters' Web of Knowledge
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