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Synthesis and structural characterisation of [Pb-5(eta-Cp-S)(4)(OSO2CF3)(6)] {Cp-S = C5Me4(SiMe2But)}
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UNSPECIFIED (2000) Synthesis and structural characterisation of [Pb-5(eta-Cp-S)(4)(OSO2CF3)(6)] {Cp-S = C5Me4(SiMe2But)}. MAIN GROUP METAL CHEMISTRY, 23 (5). pp. 307-310. ISSN 0334-7575
Full text not available from this repository.Abstract
The preparation and characterisation of [Pb-5(eta-Cp-S)(4)(OSO2CF3)(6)] 1 obtained by reacting [Pb(eta-Cp-S)(2)] with HOSO2CF3 is described in this paper [Cp-S = C5Me4(SiMe2Bu1)]. The single crystal X-ray study revealed that 1 exists as a polyionic species formed by the aggregation of four molecules of Pb(eta-Cp-S)(+) with one of Pb(OSO2CF3)(6)(4-). Compound 1 was micro-analyzed and studied by solution-state multinuclear NMR spectroscopy and the results are presented and discussed.
| Item Type: | Journal Article |
|---|---|
| Subjects: | Q Science > QD Chemistry |
| Journal or Publication Title: | MAIN GROUP METAL CHEMISTRY |
| Publisher: | FREUND PUBLISHING HOUSE LTD |
| ISSN: | 0334-7575 |
| Date: | May 2000 |
| Volume: | 23 |
| Number: | 5 |
| Number of Pages: | 4 |
| Page Range: | pp. 307-310 |
| Publication Status: | Published |
| URI: | http://wrap.warwick.ac.uk/id/eprint/13337 |
Data sourced from Thomson Reuters' Web of Knowledge
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