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Perovskite oxides rpepared by hydrothermal and solvothermal synthesis : a review of crystallisation, chemistry, and compositions

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Walton, Richard I. (2020) Perovskite oxides rpepared by hydrothermal and solvothermal synthesis : a review of crystallisation, chemistry, and compositions. Chemistry - A European Journal, 26 (42). pp. 9041-9069. doi:10.1002/chem.202000707

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Official URL: http://dx.doi.org/10.1002/chem.202000707

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Abstract

Perovskite oxides with general composition ABO3 are a large group of inorganic materials that can contain a variety of cations from all parts of the Periodic Table and that have diverse properties of application in fields ranging from electronics, energy storage to photocatalysis. Solvothermal synthesis routes to these materials have become increasingly investigated in the past decade as a means of direct crystallisation of the solids from solution. These methods have significant advantages leading to adjustment of crystal form from the nanoscale to the micron‐scale, the isolation of compositions not possible using conventional solid‐state synthesis and in addition may lead to scalable processes for producing materials at moderate temperatures. These aspects are reviewed, with examples taken from the past decade’s literature on the solvothermal synthesis of perovskites with a systematic survey of B‐site cations, from transition metals in Groups 4‐8 and main group elements in Groups 13, 14 and 15, to solid solutions and heterostructures. As well as hydrothermal reactions, the use of various solvents and solution additives are discussed and some trends identified, along with prospects for developing control and predictability in the crystallisation of complex oxide materials.

Item Type: Journal Article
Subjects: Q Science > QD Chemistry
Q Science > QE Geology
Divisions: Faculty of Science > Chemistry
Library of Congress Subject Headings (LCSH): Perovskite , Oxide minerals, Perovskite -- Effect of high temperatures on , High temperature chemistry, Crystallization
Journal or Publication Title: Chemistry - A European Journal
Publisher: Wiley - V C H Verlag GmbH & Co. KGaA
ISSN: 0947-6539
Official Date: 27 July 2020
Dates:
DateEvent
27 July 2020Published
8 April 2020Available
8 April 2020Accepted
Volume: 26
Number: 42
Page Range: pp. 9041-9069
DOI: 10.1002/chem.202000707
Status: Peer Reviewed
Publication Status: Published
Publisher Statement: "This is the peer reviewed version of the following article: Walton, R..I. (2020), Perovskite Oxides Prepared by Hydrothermal and Solvothermal Synthesis: a Review of Crystallisation, Chemistry, and Compositions. Chem. Eur. J.. Accepted Author Manuscript. doi:10.1002/chem.202000707 which has been published in final form at http://dx.doi.org/10.1002/chem.202000707. This article may be used for non-commercial purposes in accordance with Wiley Terms and Conditions for Use of Self-Archived Versions."
Access rights to Published version: Restricted or Subscription Access
RIOXX Funder/Project Grant:
Project/Grant IDRIOXX Funder NameFunder ID
UNSPECIFIEDRoyal Society of Chemistryhttp://dx.doi.org/10.13039/501100000704

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