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The square-pyramidal Pd-II complex of a cross-bridged tetraazamacrocycle
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UNSPECIFIED (1999) The square-pyramidal Pd-II complex of a cross-bridged tetraazamacrocycle. ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 55 (Part 9). pp. 1404-1406. ISSN 0108-2701
Full text not available from this repository.Abstract
The preparation and crystal structure of chloro(4,11-dimethyl-1,4, 8,11-tetraazabicyclo[6.6.2]hexadecane-kappa(4)N)palladium(II) chloride dihydrate, [PdCl(C14H30N4)]CI . 2H(2)O, are described. The Pd-II ion is coordinated to all four N atoms of the folded macrobicycle and to a single chloride ligand in a square-pyramidal geometry. The bond to the axial N atom is considerably longer than the others [Pd-N-ax 2.461 (3) and average Pd-N-eq 2.097 (10) Angstrom]. The Pd-Cl distance is 2.3407 (10) Angstrom.
| Item Type: | Journal Article |
|---|---|
| Subjects: | Q Science > QD Chemistry |
| Journal or Publication Title: | ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS |
| Publisher: | MUNKSGAARD INT PUBL LTD |
| ISSN: | 0108-2701 |
| Date: | 15 September 1999 |
| Volume: | 55 |
| Number: | Part 9 |
| Number of Pages: | 3 |
| Page Range: | pp. 1404-1406 |
| Publication Status: | Published |
| URI: | http://wrap.warwick.ac.uk/id/eprint/14138 |
Data sourced from Thomson Reuters' Web of Knowledge
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