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Simultaneous MQMAS NMR experiments for two half-integer quadrupolar nuclei

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Page, Samuel J., Gallo, Angelo, Brown, Steven P., Lewandowski, Józef R., Hanna, John V. and Franks, W. Trent (2020) Simultaneous MQMAS NMR experiments for two half-integer quadrupolar nuclei. Journal of Magnetic Resonance, 320 . 106831. doi:10.1016/j.jmr.2020.106831

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Official URL: https://doi.org/10.1016/j.jmr.2020.106831

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Abstract

A procedure to acquire two Multiple-Quantum Magic Angle Spinning (MQMAS) NMR experiments with the same instrument time is presented. A triply tuned probe is utilized with multiple receivers to collect data with staggered acquisitions and thus more efficiently use the instrument time. The data for one nucleus is collected during the recovery delay of the other nucleus, and vice versa. The instrument time is reduced to 60-80% of the time needed for the single acquisition collection Specifically our approach is presented for recording triple-quantum (3Q) 17O and either 3Q or quintuple-quantum (5Q) 27Al MAS NMR spectra of a 1.18Na2O•5SiO2•Al2O3 glass gel.

Item Type: Journal Article
Subjects: Q Science > QC Physics
Divisions: Faculty of Science > Chemistry
Faculty of Science > Physics
SWORD Depositor: Library Publications Router
Library of Congress Subject Headings (LCSH): Nuclear magnetic resonance spectroscopy, Nuclear quadrupole resonance spectroscopy, Nuclear magnetic resonance, Nuclear quadrupole resonance
Journal or Publication Title: Journal of Magnetic Resonance
Publisher: Academic Press
ISSN: 1090-7807
Official Date: November 2020
Dates:
DateEvent
November 2020Published
23 September 2020Available
18 September 2020Accepted
Volume: 320
Article Number: 106831
DOI: 10.1016/j.jmr.2020.106831
Status: Peer Reviewed
Publication Status: Published
Access rights to Published version: Open Access
RIOXX Funder/Project Grant:
Project/Grant IDRIOXX Funder NameFunder ID
FP/2007-2013/ERC Grant Agreement 639907Seventh Framework Programmehttp://dx.doi.org/10.13039/100011102
BB/L022761/1 [BBSRC] Biotechnology and Biological Sciences Research Councilhttp://dx.doi.org/10.13039/501100000268
BB/R010218/1[BBSRC] Biotechnology and Biological Sciences Research Councilhttp://dx.doi.org/10.13039/501100000268
KTP10904Innovate UKhttp://dx.doi.org/10.13039/501100006041
PR140003[EPSRC] Engineering and Physical Sciences Research Councilhttp://dx.doi.org/10.13039/501100000266
PR140003[BBSRC] Biotechnology and Biological Sciences Research Councilhttp://dx.doi.org/10.13039/501100000268
UNSPECIFIEDAdvantage West Midlandshttp://dx.doi.org/10.13039/100014381
UNSPECIFIED[ERDF] European Regional Development Fundhttp://dx.doi.org/10.13039/501100008530
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