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Extraction of vanillin following bioconversion of rice straw and its optimization by response surface methodology
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Nurika, Irnia, Suhartini, Sri, Azizah, Nurul and Barker, Guy C. (2020) Extraction of vanillin following bioconversion of rice straw and its optimization by response surface methodology. Molecules, 25 (24). e6031. doi:10.3390/molecules25246031 ISSN 1420-3049.
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WRAP-Extraction-vanillin-following-bioconversion-rice-straw-optimization-2020.pdf - Published Version - Requires a PDF viewer. Available under License Creative Commons Attribution 4.0. Download (3079Kb) | Preview |
Official URL: https://doi.org/10.3390/molecules25246031
Abstract
Value-added chemicals, including phenolic compounds, can be generated through lignocellulosic biomass conversion via either biological or chemical pretreatment. Currently vanillin is one of the most valuable of these products that has been shown to be extractable on an industrial scale. This study demonstrates the potential of using rice straw inoculated with Serpula lacrymans, which produced a mixture of high value bio-based compounds including vanillin. Key extraction conditions were identified to be the volume of solvent used and extraction time, which were optimized using response surface methodology (RSM). The vanillin compounds extracted from rice straw solid state fermentation (SSF) was confirmed through LC-ESI MS/MS in selective ion mode. The optimum concentration and yield differed depending on the solvent, which was predicted using 60 mL ethyl acetate for 160 min were 0.408% and 3.957 μg g−1 respectively. In comparison, when ethanol was used, the highest concentration and yields of vanillin were 0.165% and 2.596 μg g−1. These were achieved using 40 mL of solvent, and extraction time increased to 248 min. The results confirm that fungal conversion of rice straw to vanillin could consequently offer a cost-effect alternative to other modes of production.
Item Type: | Journal Article | |||||||||
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Subjects: | Q Science > QD Chemistry Q Science > QK Botany S Agriculture > SB Plant culture T Technology > TP Chemical technology |
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Divisions: | Faculty of Science, Engineering and Medicine > Science > Life Sciences (2010- ) | |||||||||
SWORD Depositor: | Library Publications Router | |||||||||
Library of Congress Subject Headings (LCSH): | Vanillin , Lignocellulose , Straw, Straw -- Utilization , Extraction (Chemistry), Serpula lacrymans, Biomass conversion | |||||||||
Journal or Publication Title: | Molecules | |||||||||
Publisher: | MDPI | |||||||||
ISSN: | 1420-3049 | |||||||||
Official Date: | 19 December 2020 | |||||||||
Dates: |
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Volume: | 25 | |||||||||
Number: | 24 | |||||||||
Article Number: | e6031 | |||||||||
DOI: | 10.3390/molecules25246031 | |||||||||
Status: | Peer Reviewed | |||||||||
Publication Status: | Published | |||||||||
Reuse Statement (publisher, data, author rights): | ** From MDPI via Jisc Publications Router ** History: accepted 17-12-2020; pub-electronic 19-12-2020. ** Licence for this article: https://creativecommons.org/licenses/by/4.0/ | |||||||||
Access rights to Published version: | Open Access (Creative Commons) | |||||||||
Date of first compliant deposit: | 21 December 2020 | |||||||||
Date of first compliant Open Access: | 22 December 2020 | |||||||||
RIOXX Funder/Project Grant: |
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