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Preparative enantioseparation on polysaccharide phase using microporous silica as a support

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UNSPECIFIED (1998) Preparative enantioseparation on polysaccharide phase using microporous silica as a support. In: 8th International Symposium on Chiral Discrimination (ISCD 97), 1997, NAGOYA, JAPAN.

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Abstract

The preparative enantiomeric resolutions of hexahelicen-7-yl acetic acid methyl ester and two sulphoxides were performed on cellulose tris(3,5-dimethylphenylcarbamate) coated onto aminopropylated 5-mu m silica with 120-Angstrom diameter pore. High enantiomeric purity was obtained for both enantiomers. The enantioselectivity of the amylose tris (3, 5-dimethylphenylcarbamate), cellule se and amylose tris (phenylcarbamate) phases for the hexahelicen-7-yl acetic acid derivative were also investigated. (C) 1998 Wiley-Liss, Inc.

Item Type: Conference Item (UNSPECIFIED)
Subjects: Q Science > QD Chemistry
R Medicine > RS Pharmacy and materia medica
Journal or Publication Title: CHIRALITY
Publisher: WILEY-LISS
ISSN: 0899-0042
Date: 1998
Volume: 10
Number: 7
Number of Pages: 5
Page Range: pp. 573-577
Publication Status: Published
Title of Event: 8th International Symposium on Chiral Discrimination (ISCD 97)
Location of Event: NAGOYA, JAPAN
Date(s) of Event: 1997
URI: http://wrap.warwick.ac.uk/id/eprint/15348

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