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NMR studies of group 8 metallodrugs : 187Os-enriched organo-osmium half-sandwich anticancer complex

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Needham, Russell J., Prokes, Ivan, Habtemariam, Abraha, Romero-Canelón, Isolda, Clarkson, Guy J. and Sadler, Peter J. (2021) NMR studies of group 8 metallodrugs : 187Os-enriched organo-osmium half-sandwich anticancer complex. Dalton Transactions, 50 (37). pp. 12970-12981. doi:10.1039/d1dt02213j

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Official URL: https://doi.org/10.1039/D1DT02213J

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Abstract

Synthesis of this 187Os-enriched organo-osmium azopyridine anticancer complex, has allowed determination of 187Os NMR J-couplings to ligand 1H and 13C, and the 187Os chemical shift. The complex was also characterised by X-ray crystallography and MS.

Item Type: Journal Article
Subjects: Q Science > QD Chemistry
Q Science > QP Physiology
R Medicine > R Medicine (General)
R Medicine > RC Internal medicine
R Medicine > RM Therapeutics. Pharmacology
Divisions: Faculty of Science > Chemistry
SWORD Depositor: Library Publications Router
Library of Congress Subject Headings (LCSH): Nuclear magnetic resonance spectroscopy, Metals in medicine, Metal complexes -- Therapeutic use, Cancer -- Treatment, Cancer -- Research, Organoosmium compounds
Journal or Publication Title: Dalton Transactions
Publisher: Royal Society of Chemistry (RSC)
ISSN: 1477-9234
Official Date: 7 October 2021
Dates:
DateEvent
7 October 2021Published
24 August 2021Available
7 August 2021Accepted
Volume: 50
Number: 37
Page Range: pp. 12970-12981
DOI: 10.1039/d1dt02213j
Status: Peer Reviewed
Publication Status: Published
Access rights to Published version: Open Access
RIOXX Funder/Project Grant:
Project/Grant IDRIOXX Funder NameFunder ID
EP/F034210/1[EPSRC] Engineering and Physical Sciences Research Councilhttp://dx.doi.org/10.13039/501100000266
EP/P030572/1 [EPSRC] Engineering and Physical Sciences Research Councilhttp://dx.doi.org/10.13039/501100000266
247450European Research Councilhttp://dx.doi.org/10.13039/501100000781
UNSPECIFIEDAnglo American Platinum Corporation Limitedhttp://viaf.org/viaf/138772564
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