Send, Sebastian, von Kozierowski, Marc, Panzner, Tobias, Gorfman, S., Nurdan, Kivanc, Walenta, Albert H., Pietsch, Ullrich, Leitenberger, Wolfram, Hartmann, Robert and Strueder, Lothar (2009) Energy-dispersive Laue diffraction by means of a frame-store pnCCD. Journal of Applied Crystallography, Vol.42 (Part 6). pp. 1139-1146. doi:10.1107/S0021889809039867

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Abstract

A frame-store pn-junction CCD detector was applied to the energy-dispersive X-ray Laue diffraction study of a gamma-LiAlO2 crystal with white synchrotron radiation. Exploiting the simultaneous spatial and energy resolution of the detector the crystallographic unit cell of gamma-LiAlO2 could be determined without any a priori information about the sample. The potential for application in X-ray structure analysis is tested by comparing experimental structure factors taken under a single exposure with those calculated from the known crystal structure. After correcting the measured spot intensities by angular and energy-dependent parameters, the agreement between experimental and theoretical kinematical structure factors is better than 10%.

Item Type:	Journal Article
Subjects:	Q Science > QD Chemistry
Divisions:	Faculty of Science > Physics
Journal or Publication Title:	Journal of Applied Crystallography
Publisher:	Wiley-Blackwell Publishing Ltd.
ISSN:	0021-8898
Official Date:	December 2009
Dates:	Date Event December 2009 Published
Volume:	Vol.42
Number:	Part 6
Number of Pages:	8
Page Range:	pp. 1139-1146
DOI:	10.1107/S0021889809039867
Status:	Peer Reviewed
Publication Status:	Published
Access rights to Published version:	Restricted or Subscription Access
Funder:	BMBF Verbundforschung
Grant number:	05KS7PSA

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