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Energy-dispersive Laue diffraction by means of a frame-store pnCCD

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Send, Sebastian, von Kozierowski, Marc, Panzner, Tobias, Gorfman, S., Nurdan, Kivanc, Walenta, Albert H., Pietsch, Ullrich, Leitenberger, Wolfram, Hartmann, Robert and Strueder, Lothar (2009) Energy-dispersive Laue diffraction by means of a frame-store pnCCD. Journal of Applied Crystallography, Vol.42 (Part 6). pp. 1139-1146. doi:10.1107/S0021889809039867

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Official URL: http://dx.doi.org/10.1107/S0021889809039867

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Abstract

A frame-store pn-junction CCD detector was applied to the energy-dispersive X-ray Laue diffraction study of a gamma-LiAlO2 crystal with white synchrotron radiation. Exploiting the simultaneous spatial and energy resolution of the detector the crystallographic unit cell of gamma-LiAlO2 could be determined without any a priori information about the sample. The potential for application in X-ray structure analysis is tested by comparing experimental structure factors taken under a single exposure with those calculated from the known crystal structure. After correcting the measured spot intensities by angular and energy-dependent parameters, the agreement between experimental and theoretical kinematical structure factors is better than 10%.

Item Type: Journal Article
Subjects: Q Science > QD Chemistry
Divisions: Faculty of Science > Physics
Journal or Publication Title: Journal of Applied Crystallography
Publisher: Wiley-Blackwell Publishing Ltd.
ISSN: 0021-8898
Official Date: December 2009
Dates:
DateEvent
December 2009Published
Volume: Vol.42
Number: Part 6
Number of Pages: 8
Page Range: pp. 1139-1146
DOI: 10.1107/S0021889809039867
Status: Peer Reviewed
Publication Status: Published
Access rights to Published version: Restricted or Subscription Access
Funder: BMBF Verbundforschung
Grant number: 05KS7PSA

Data sourced from Thomson Reuters' Web of Knowledge

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