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Slice & Dice : nested spin–lattice relaxation measurements
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Franks, W. Trent, Tognetti, Jacqueline and Lewandowski, Józef R. (2023) Slice & Dice : nested spin–lattice relaxation measurements. Physical Chemistry Chemical Physics . doi:10.1039/d2cp03458a ISSN 1463-9084. (In Press)
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Official URL: https://doi.org/10.1039/d2cp03458a
Abstract
Spin–lattice relaxation rate (R1) measurements are commonly used to characterize protein dynamics. However, the time needed to collect the data can be quite long due to long relaxation times of the low-gamma nuclei, especially in the solid state. We present a method to collect backbone heavy atom relaxation data by nesting the collection of datasets in the solid state. This method results in a factor of 2 to 2.5 times faster data acquisition for backbone R1 relaxation data for the 13C and 15N sites of proteins.
| Item Type: | Journal Article | |||||||||||||||
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| Subjects: | Q Science > QC Physics Q Science > QD Chemistry Q Science > QP Physiology |
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| Divisions: | Faculty of Science, Engineering and Medicine > Science > Chemistry Faculty of Science, Engineering and Medicine > Science > Physics |
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| SWORD Depositor: | Library Publications Router | |||||||||||||||
| Library of Congress Subject Headings (LCSH): | Spin excitations, Proteins -- Analysis, Nuclear magnetic resonance spectroscopy | |||||||||||||||
| Journal or Publication Title: | Physical Chemistry Chemical Physics | |||||||||||||||
| Publisher: | Royal Society of Chemistry (RSC) | |||||||||||||||
| ISSN: | 1463-9084 | |||||||||||||||
| Official Date: | 2023 | |||||||||||||||
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| DOI: | 10.1039/d2cp03458a | |||||||||||||||
| Status: | Peer Reviewed | |||||||||||||||
| Publication Status: | In Press | |||||||||||||||
| Access rights to Published version: | Open Access (Creative Commons) | |||||||||||||||
| Date of first compliant deposit: | 9 December 2022 | |||||||||||||||
| Date of first compliant Open Access: | 9 December 2022 | |||||||||||||||
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