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One-step synthesis of fullerene hydride C60H2 via hydrolysis of acylated fullerenes
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Tzirakis, Manolis D., Alberti, Mariza N., Nye, Leanne C., Drewello, Thomas and Orfanopoulos, Michael. (2009) One-step synthesis of fullerene hydride C60H2 via hydrolysis of acylated fullerenes. Journal of Organic Chemistry, Vol.74 (No.15). pp. 5746-5749. ISSN 0022-3263
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Official URL: http://dx.doi.org/10.1021/jo900934j
Abstract
The hitherto unexplored class of acylated fullerene compounds has been shown to be excellent C60H2 precursors. Upon a simple treatment with basic Al2O3, they are hydrolyzed quantitatively into C60H2, This key feature led to the development of a new, straightforward protocol for the selective synthesis of the simplest [60] fullerene hydride, C60H2. This protocol may offer an advantageous alternative to previously known methods for the synthesis of C60H2 allowing for a rapid access to C60H2 in good yield and high purity without tedious separating processes.
| Item Type: | Journal Article |
|---|---|
| Subjects: | Q Science > QD Chemistry |
| Divisions: | Faculty of Science > Chemistry |
| Journal or Publication Title: | Journal of Organic Chemistry |
| Publisher: | American Chemical Society |
| ISSN: | 0022-3263 |
| Date: | 7 August 2009 |
| Volume: | Vol.74 |
| Number: | No.15 |
| Number of Pages: | 4 |
| Page Range: | pp. 5746-5749 |
| Identification Number: | 10.1021/jo900934j |
| Status: | Peer Reviewed |
| Publication Status: | Published |
| Access rights to Published version: | Restricted or Subscription Access |
| Funder: | The Greek National Scholarships Foundation (IKY) |
| URI: | http://wrap.warwick.ac.uk/id/eprint/17514 |
Data sourced from Thomson Reuters' Web of Knowledge
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