Single-crystal K-x(ZnyTi8-y)O-16 priderites: Growth and characterization
UNSPECIFIED (1996) Single-crystal K-x(ZnyTi8-y)O-16 priderites: Growth and characterization. JOURNAL OF MATERIALS SCIENCE, 31 (24). pp. 6463-6468. ISSN 0022-2461Full text not available from this repository.
Single crystals of K-x(ZnyTi8-y)O-16 priderites have been grown from a melt of K2O-MoO3 using the flux-zone technique. High-purity crystals > 10 mm in length were obtained, with no indication of twinning. Lattice parameters of a=1.0162(8) nm and c=0.2971(7) nm were obtained from X-ray diffraction measurements. Habit planes were identified from scanning electron microscope images. X-ray photoelectron spectroscopy confirmed the titanium oxidation state as +4. High-temperature complex impedance spectroscopy between 300 and 820 K was used to electrically characterize the crystals. This indicated that the materials had a low d.c. conductivity and a conductivity of 1.68 x 10(-3) S cm(-1) at 100 kHz.
|Item Type:||Journal Article|
|Subjects:||T Technology > TA Engineering (General). Civil engineering (General)|
|Journal or Publication Title:||JOURNAL OF MATERIALS SCIENCE|
|Publisher:||CHAPMAN HALL LTD|
|Date:||15 December 1996|
|Number of Pages:||6|
|Page Range:||pp. 6463-6468|
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