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An X-ray diffraction and NMR study into the mechanism of zircon formation from aqueous sols
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UNSPECIFIED (1996) An X-ray diffraction and NMR study into the mechanism of zircon formation from aqueous sols. JOURNAL OF MATERIALS SCIENCE, 31 (22). pp. 5873-5876. ISSN 0022-2461
Full text not available from this repository.Abstract
Solid solutions of the formula Zr1-xSixO2 (x=0-0.5) were produced by an aqueous inorganic set-gel route. X-ray diffraction and solid state magic-angle spinning-nuclear magnetic resonance (MAS-NMR) were used to characterize the products at various calcination temperatures. The solubility limit of silica in zirconia at <950 degrees C was found to be similar to x=0.15 and that this amount stabilized the tetragonal zirconia phase to higher temperatures and inhibited the formation of zircon. With x=0.5, zircon formation was 70% at only 1100 degrees C.
| Item Type: | Journal Article |
|---|---|
| Subjects: | T Technology > TA Engineering (General). Civil engineering (General) |
| Journal or Publication Title: | JOURNAL OF MATERIALS SCIENCE |
| Publisher: | CHAPMAN HALL LTD |
| ISSN: | 0022-2461 |
| Date: | 15 November 1996 |
| Volume: | 31 |
| Number: | 22 |
| Number of Pages: | 4 |
| Page Range: | pp. 5873-5876 |
| Publication Status: | Published |
| URI: | http://wrap.warwick.ac.uk/id/eprint/18198 |
Data sourced from Thomson Reuters' Web of Knowledge
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