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HYDRORUTHENATION OF PROP-2-YNYLTRIPHENYLPHOSPHONIUM BROMIDE - SYNTHESIS, CRYSTAL-STRUCTURE AND REACTIONS OF [RUBR(CH=CHCH(2)PPH(3))(CO)(PPH(3))(2)]PF6
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UNSPECIFIED (1995) HYDRORUTHENATION OF PROP-2-YNYLTRIPHENYLPHOSPHONIUM BROMIDE - SYNTHESIS, CRYSTAL-STRUCTURE AND REACTIONS OF [RUBR(CH=CHCH(2)PPH(3))(CO)(PPH(3))(2)]PF6. JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS (3). pp. 369-370. ISSN 0022-4936.
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Abstract
The reaction of the complex [RuClH(CO)(PPh(3))(3)] with prop-2-ynyltriphenylphosphonium bromide ([Ph(3)PCH(2)C equivalent to CH]Br) followed by NH4PF6 provides the crystallographically characterised salt [RuBr(CH=CHCH(2)PPh(3))(CO)(PPh(3))(2)]PF6 which by virtue of the coordinative unsaturation at the ruthenium centre undergoes addition of the ligands CNC(6)H(3)Me(2)-2,6, and CO to Ru and insertion of SO2 into the Ru-C sigma-bond.
Item Type: | Journal Article | ||||
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Subjects: | Q Science > QD Chemistry | ||||
Journal or Publication Title: | JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS | ||||
Publisher: | ROYAL SOC CHEMISTRY | ||||
ISSN: | 0022-4936 | ||||
Official Date: | 7 February 1995 | ||||
Dates: |
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Number: | 3 | ||||
Number of Pages: | 2 | ||||
Page Range: | pp. 369-370 | ||||
Publication Status: | Published |
Data sourced from Thomson Reuters' Web of Knowledge
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