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MONOCHLOROINDIUM DERIVATIVE OF TMTAA (DIBENZOTETRAMETHYLTETRAAZA[14]ANNULENE), [IN(C22H22N4)CL]

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UNSPECIFIED (1994) MONOCHLOROINDIUM DERIVATIVE OF TMTAA (DIBENZOTETRAMETHYLTETRAAZA[14]ANNULENE), [IN(C22H22N4)CL]. ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 50 (Part 7). pp. 1072-1074.

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Abstract

The structure consists of an InCl fragment bonded symmetrically to the four N atoms of the macrocyclic ligand tmtaa (chloro{3,5,14,16-tetramethyl-2,6,13,17-tetraaza-tricyclo[16.4.0.0(7,12)]docosa-1(18),2,5,7(12),8,10,13,16,-19,21-decaenediido-N,N,N'',N'''}indium). This is the first structural characterization of an In entity coordinated to this ligand and reveals an unusual five-coordinate square-pyramidal geometry around the In atom. The metal is displaced 0.738 (3) angstrom above the N4 coordination plane. The average In-N bond distance is 2.165 (5) angstrom and the In-Cl distance is 2.380 angstrom.

Item Type: Journal Article
Subjects: Q Science > QD Chemistry
Journal or Publication Title: ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS
Publisher: MUNKSGAARD INT PUBL LTD
ISSN: 0108-2701
Official Date: 15 July 1994
Dates:
DateEvent
15 July 1994UNSPECIFIED
Volume: 50
Number: Part 7
Number of Pages: 3
Page Range: pp. 1072-1074
Publication Status: Published

Data sourced from Thomson Reuters' Web of Knowledge

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