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CHIRAL HPLC WITH CARBOHYDRATE CARBAMATES - INFLUENCE OF SUPPORT STRUCTURE ON ENANTIOSELECTIVITY
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UNSPECIFIED (1994) CHIRAL HPLC WITH CARBOHYDRATE CARBAMATES - INFLUENCE OF SUPPORT STRUCTURE ON ENANTIOSELECTIVITY. In: 4th International Symposium on Chiral Discrimination (4th-ISCD), SEP 19-22, 1993, MONTREAL, CANADA.
Full text not available from this repository.Abstract
The effect of particle size and pore size of the aminopropylated silica support for cellulose tris(phenylcarbamate) and tris(3,5-dimethylphenylcarbamate) chiral HPLC phases was investigated. It was necessary to reduce phase loading below 20% w/w as pore size and particle size were reduced, but high efficiency columns could be prepared at a 15% w/w loading on 5 and 2.5 mu m supports with 120-Angstrom-diameter pores. The 2.5 mu m phase permits the use of relatively high flow rates and very efficient enantioselective separations of a range of chiral compounds could be achieved in less than 3 min. (C) 1994 Wiley-Liss, Inc.
| Item Type: | Conference Item (UNSPECIFIED) |
|---|---|
| Subjects: | Q Science > QD Chemistry R Medicine > RS Pharmacy and materia medica |
| Journal or Publication Title: | CHIRALITY |
| Publisher: | WILEY-LISS |
| ISSN: | 0899-0042 |
| Date: | 1994 |
| Volume: | 6 |
| Number: | 2 |
| Number of Pages: | 6 |
| Page Range: | pp. 129-134 |
| Publication Status: | Published |
| Title of Event: | 4th International Symposium on Chiral Discrimination (4th-ISCD) |
| Location of Event: | MONTREAL, CANADA |
| Date(s) of Event: | SEP 19-22, 1993 |
| URI: | http://wrap.warwick.ac.uk/id/eprint/20696 |
Data sourced from Thomson Reuters' Web of Knowledge
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