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CHIRAL HPLC WITH CARBOHYDRATE CARBAMATES - INFLUENCE OF SUPPORT STRUCTURE ON ENANTIOSELECTIVITY
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UNSPECIFIED (1994) CHIRAL HPLC WITH CARBOHYDRATE CARBAMATES - INFLUENCE OF SUPPORT STRUCTURE ON ENANTIOSELECTIVITY. In: 4th International Symposium on Chiral Discrimination (4th-ISCD), MONTREAL, CANADA, SEP 19-22, 1993. Published in: CHIRALITY, 6 (2). pp. 129-134. ISSN 0899-0042.
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Abstract
The effect of particle size and pore size of the aminopropylated silica support for cellulose tris(phenylcarbamate) and tris(3,5-dimethylphenylcarbamate) chiral HPLC phases was investigated. It was necessary to reduce phase loading below 20% w/w as pore size and particle size were reduced, but high efficiency columns could be prepared at a 15% w/w loading on 5 and 2.5 mu m supports with 120-Angstrom-diameter pores. The 2.5 mu m phase permits the use of relatively high flow rates and very efficient enantioselective separations of a range of chiral compounds could be achieved in less than 3 min. (C) 1994 Wiley-Liss, Inc.
Item Type: | Conference Item (UNSPECIFIED) | ||||
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Subjects: | Q Science > QD Chemistry R Medicine > RS Pharmacy and materia medica |
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Journal or Publication Title: | CHIRALITY | ||||
Publisher: | WILEY-LISS | ||||
ISSN: | 0899-0042 | ||||
Official Date: | 1994 | ||||
Dates: |
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Volume: | 6 | ||||
Number: | 2 | ||||
Number of Pages: | 6 | ||||
Page Range: | pp. 129-134 | ||||
Publication Status: | Published | ||||
Title of Event: | 4th International Symposium on Chiral Discrimination (4th-ISCD) | ||||
Location of Event: | MONTREAL, CANADA | ||||
Date(s) of Event: | SEP 19-22, 1993 |
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