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BIS(ETA(5)-TERT-BUTYLCYCLOPENTADIENYL)DICHLORONIOBIUM(IV)

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UNSPECIFIED (1994) BIS(ETA(5)-TERT-BUTYLCYCLOPENTADIENYL)DICHLORONIOBIUM(IV). ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 50 (Part 1). pp. 33-36.

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Abstract

The monomeric molecule of the title compound, [NbCl2-(C9H13)2], is best described as a paramagnetic pseudo-tetrahedral complex of niobium(IV). The two tert-butylcyclopentadienyl ligands are asymmetrically bound to the Nb atom [Nb-C bond-length range 2.394 (6)-2.470 (6) angstrom]. The asymmetry is accounted for in terms of the steric demand of the (t)Bu groups and Cl ligands. Pseudo-tetrahedral geometry is completed by two Cl ligands [Nb-Cl 2.477 (2) and 2.483 (2) angstrom, Cl-Nb-Cl 84.15 (6)-degrees].

Item Type: Journal Article
Subjects: Q Science > QD Chemistry
Journal or Publication Title: ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS
Publisher: MUNKSGAARD INT PUBL LTD
ISSN: 0108-2701
Official Date: 15 January 1994
Dates:
DateEvent
15 January 1994UNSPECIFIED
Volume: 50
Number: Part 1
Number of Pages: 4
Page Range: pp. 33-36
Publication Status: Published

Data sourced from Thomson Reuters' Web of Knowledge

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