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SYNTHETIC, SPECTROSCOPIC AND X-RAY CRYSTALLOGRAPHIC STUDIES ON COMPLEXES FORMED BETWEEN INDIUM(III) IODIDE AND PHOSPHINE-LIGANDS
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UNSPECIFIED (1992) SYNTHETIC, SPECTROSCOPIC AND X-RAY CRYSTALLOGRAPHIC STUDIES ON COMPLEXES FORMED BETWEEN INDIUM(III) IODIDE AND PHOSPHINE-LIGANDS. JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS (19). pp. 2775-2780. ISSN 0300-9246.
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Abstract
The 1 : 1 adducts of InI3 with various phosphine ligands [PR3; R3 = Bu(i)3, HPh2, HBut2 or H(C6H11)2 (C6H11 = cyclohexyl)] have been prepared and characterised, and their solution properties, as examined by H-1, P-31 and In-115 NMR and conductivity measurements, indicate the presence of only neutral species. Infrared and Raman data have been recorded for the adducts in the solid state and compared with other published data. X-Ray studies on InI.PHR2 (R = Ph or Bu(t)) confirm the presence of neutral compounds containing four-co-ordinate indium atoms, but reveal that significant intermolecular interactions (In-I-In, P-H-I, In-I-I-In) are present.
Item Type: | Journal Article | ||||
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Subjects: | Q Science > QD Chemistry | ||||
Journal or Publication Title: | JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS | ||||
Publisher: | ROYAL SOC CHEMISTRY | ||||
ISSN: | 0300-9246 | ||||
Official Date: | 7 October 1992 | ||||
Dates: |
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Number: | 19 | ||||
Number of Pages: | 6 | ||||
Page Range: | pp. 2775-2780 | ||||
Publication Status: | Published |
Data sourced from Thomson Reuters' Web of Knowledge
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