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RUTHENATETRABORANES - SYNTHESIS OF [RU(B3H8)(PPH3)(HB(PZ)3)] AND CRYSTAL-STRUCTURE OF [RUCL(PPH3)2(HB(PZ)3)] (PZ = PYRAZOL-1-YL)
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UNSPECIFIED (1992) RUTHENATETRABORANES - SYNTHESIS OF [RU(B3H8)(PPH3)(HB(PZ)3)] AND CRYSTAL-STRUCTURE OF [RUCL(PPH3)2(HB(PZ)3)] (PZ = PYRAZOL-1-YL). INORGANIC CHEMISTRY, 31 (13). pp. 2906-2908. ISSN 0020-1669.
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Abstract
The reaction of [RuCl2(PPh3)3] with K[HB(pz)3] (pz = pyrazol-1-yl) affords [RuCl(PPhl)2{kappa-3-HB(pz)3}] [crystallographically characterized with monoclinic crystals of space group P2(1)/a, Z = 8, in a unit cell of dimensions a = 19.75 (1) angstrom, b = 22.48 (1) angstrom, c = 20.283 (7) angstrom, and beta = 112.94 (3)-degrees], which upon treatment with NR4[B3H8] (R = Me, Bu) provides the ruthenatetraborane [Ru(B3H8)(PPh3){kappa-3-HB(pz)3}].
Item Type: | Journal Article | ||||
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Subjects: | Q Science > QD Chemistry | ||||
Journal or Publication Title: | INORGANIC CHEMISTRY | ||||
Publisher: | AMER CHEMICAL SOC | ||||
ISSN: | 0020-1669 | ||||
Official Date: | 24 June 1992 | ||||
Dates: |
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Volume: | 31 | ||||
Number: | 13 | ||||
Number of Pages: | 3 | ||||
Page Range: | pp. 2906-2908 | ||||
Publication Status: | Published |
Data sourced from Thomson Reuters' Web of Knowledge
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