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A Co-59 NMR study to observe the effects of ball milling on small ferromagnetic cobalt particles
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Speight, R. J. (Richard J.), Wong, Alan, Ellis, P., Hyde, T., Bishop, P. T. and Smith, Mark E. (2009) A Co-59 NMR study to observe the effects of ball milling on small ferromagnetic cobalt particles. Solid State Nuclear Magnetic Resonance, Vol.35 (No.2). pp. 67-73. doi:10.1016/j.ssnmr.2008.12.001 ISSN 0926-2040.
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Official URL: http://dx.doi.org/10.1016/j.ssnmr.2008.12.001
Abstract
To demonstrate the potential of nuclear magnetic resonance (NMR) spectroscopy for investigating detailed structural properties in ferromagnetic materials, three different particle sized cobalt (Co) powders have been ball milled for 24 h are accurately characterised by internal-field Co-59 NMR. The Co-59 NMR spectra show distinct resonance bands corresponding to the different Co sites. face-centred-cubic (fcc), hexagonal-close-packed (hcp) and stacking faults (sfs), in Co metal powders. The hcp+fcc-->hcp phase transition encouraged by ball-milling was observed and quantitative values for each Co environment were obtained. (C) 2008 Elsevier Inc. All rights reserved.
| Item Type: | Journal Article | ||||
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| Subjects: | Q Science > QD Chemistry Q Science > QC Physics |
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| Divisions: | Administration > University Executive Office Faculty of Science, Engineering and Medicine > Science > Physics |
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| Journal or Publication Title: | Solid State Nuclear Magnetic Resonance | ||||
| Publisher: | Academic Press | ||||
| ISSN: | 0926-2040 | ||||
| Official Date: | April 2009 | ||||
| Dates: |
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| Volume: | Vol.35 | ||||
| Number: | No.2 | ||||
| Number of Pages: | 7 | ||||
| Page Range: | pp. 67-73 | ||||
| DOI: | 10.1016/j.ssnmr.2008.12.001 | ||||
| Status: | Peer Reviewed | ||||
| Publication Status: | Published | ||||
| Access rights to Published version: | Restricted or Subscription Access | ||||
| Funder: | Engineering and Physical Sciences Research Council (EPSRC), Biotechnology and Biological Sciences Research Council (Great Britain) (BBSRC), Natural Sciences and Engineering Research Council of Canada NSERC, University of Warwick |
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