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Identification of phases in partially crystallised Ti-, Sr- and Zn-containing sodium calcium phosphates by two-dimensional NMR
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O'Dell, L. A., Abou Neel, Ensanya A., Knowles, Jonathan C. and Smith, Mark E. (2009) Identification of phases in partially crystallised Ti-, Sr- and Zn-containing sodium calcium phosphates by two-dimensional NMR. Materials Chemistry and Physics, Vol.114 (No.2-3). pp. 1008-1015. doi:10.1016/j.matchemphys.2008.11.002
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Official URL: http://dx.doi.org/10.1016/j.matchemphys.2008.11.00...
Abstract
P-31 and Na-23 one-dimensional MAS NMR, as well as two-dimensional P-31 refocused INADEQUATE and Na-23 multiple quantum (MQ) MAS, experiments have been used in combination with powder XRD to identify various phases present in three metal-containing sodium calcium phosphate ceramics of interest as potential biomaterials. Each sample is shown to consist of multiple phases (at least seven in the case of the Zn-containing sample), several of which were identified by NMR, but not by XRD. Solid-state NMR is thus demonstrated to be an important characterisation tool in studying multi-phase phosphate ceramics, especially those containing a mixture of crystalline and amorphous components. (C) 2008 Elsevier B.V. All rights reserved.
| Item Type: | Journal Article | ||||
|---|---|---|---|---|---|
| Subjects: | T Technology > TA Engineering (General). Civil engineering (General) | ||||
| Divisions: | Administration > Vice Chancellor's Office Faculty of Science > Physics |
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| Journal or Publication Title: | Materials Chemistry and Physics | ||||
| Publisher: | Elsevier Science SA | ||||
| ISSN: | 0254-0584 | ||||
| Official Date: | 15 April 2009 | ||||
| Dates: |
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| Volume: | Vol.114 | ||||
| Number: | No.2-3 | ||||
| Number of Pages: | 8 | ||||
| Page Range: | pp. 1008-1015 | ||||
| DOI: | 10.1016/j.matchemphys.2008.11.002 | ||||
| Status: | Peer Reviewed | ||||
| Publication Status: | Published | ||||
| Access rights to Published version: | Restricted or Subscription Access | ||||
| Funder: | Engineering and Physical Sciences Research Council (EPSRC) | ||||
| Grant number: | EP/C004698/1 (EPSRC), EP/C000714/1 (EPSRC), EP/C000633/1 (EPSRC), EP/C515560/1 (EPSRC) |
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