O'Dell, L. A., Abou Neel, Ensanya A., Knowles, Jonathan C. and Smith, Mark E.. (2009) Identification of phases in partially crystallised Ti-, Sr- and Zn-containing sodium calcium phosphates by two-dimensional NMR. Materials Chemistry and Physics, Vol.114 (No.2-3). pp. 1008-1015. ISSN 0254-0584

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Abstract

P-31 and Na-23 one-dimensional MAS NMR, as well as two-dimensional P-31 refocused INADEQUATE and Na-23 multiple quantum (MQ) MAS, experiments have been used in combination with powder XRD to identify various phases present in three metal-containing sodium calcium phosphate ceramics of interest as potential biomaterials. Each sample is shown to consist of multiple phases (at least seven in the case of the Zn-containing sample), several of which were identified by NMR, but not by XRD. Solid-state NMR is thus demonstrated to be an important characterisation tool in studying multi-phase phosphate ceramics, especially those containing a mixture of crystalline and amorphous components. (C) 2008 Elsevier B.V. All rights reserved.

Item Type:	Journal Article
Subjects:	T Technology > TA Engineering (General). Civil engineering (General)
Divisions:	Administration > Vice Chancellor's Office Faculty of Science > Physics
Journal or Publication Title:	Materials Chemistry and Physics
Publisher:	Elsevier Science SA
ISSN:	0254-0584
Official Date:	15 April 2009
Volume:	Vol.114
Number:	No.2-3
Number of Pages:	8
Page Range:	pp. 1008-1015
Identification Number:	10.1016/j.matchemphys.2008.11.002
Status:	Peer Reviewed
Publication Status:	Published
Access rights to Published version:	Restricted or Subscription Access
Funder:	Engineering and Physical Sciences Research Council (EPSRC)
Grant number:	EP/C004698/1 (EPSRC), EP/C000714/1 (EPSRC), EP/C000633/1 (EPSRC), EP/C515560/1 (EPSRC)
URI:	http://wrap.warwick.ac.uk/id/eprint/28377

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