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A natural abundance Se-77 solid-state NMR study of inorganic compounds
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Kemp, Thomas F., Wong, A. (Alan), Smith, Mark E., Bishop, P. T. and Carthey, N. (2008) A natural abundance Se-77 solid-state NMR study of inorganic compounds. Solid State Nuclear Magnetic Resonance, Volume 34 (Number 4). pp. 224-227. doi:10.1016/j.ssnmr.2008.10.003 ISSN 0926-2040.
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Official URL: http://dx.doi.org/10.1016/j.ssnmr.2008.10.003
Abstract
Various inorganic selenium-based compounds were analysed by Se-77 solid-state NMR, and a distinct difference in chemical shift ranges for compounds where selenium is present as selenide (Se2-) ionically and covalently bonded systems was observed. The selenides exhibit a shift range of approximately -700 to -100 ppm, as opposed to 700 to 1600 ppm for the Compounds where there tends to be more direct covalent bonding to the selenium. The anisotropic hyperfine shift observed in NbSe2 is shown to be axially symmetric, where the Hit component is found to be normal to the Se3-trigonal plane. (c) 2008 Elsevier Inc. All rights reserved.
| Item Type: | Journal Article | ||||
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| Subjects: | Q Science > QD Chemistry Q Science > QC Physics |
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| Divisions: | Administration > University Executive Office Faculty of Science, Engineering and Medicine > Science > Physics |
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| Library of Congress Subject Headings (LCSH): | Selenium compounds -- Spectra, Nuclear magnetic resonance spectroscopy, Hyperfine interactions, Inorganic compounds -- Analysis | ||||
| Journal or Publication Title: | Solid State Nuclear Magnetic Resonance | ||||
| Publisher: | Academic Press | ||||
| ISSN: | 0926-2040 | ||||
| Official Date: | November 2008 | ||||
| Dates: |
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| Volume: | Volume 34 | ||||
| Number: | Number 4 | ||||
| Number of Pages: | 4 | ||||
| Page Range: | pp. 224-227 | ||||
| DOI: | 10.1016/j.ssnmr.2008.10.003 | ||||
| Status: | Peer Reviewed | ||||
| Publication Status: | Published | ||||
| Access rights to Published version: | Restricted or Subscription Access | ||||
| Funder: | Engineering and Physical Sciences Research Council (EPSRC) |
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