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Control of polymorphism in NaNbO3 by hydrothermal synthesis
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Modeshia, Deena R., Darton, Richard J., Ashbrook, Sharon E. and Walton, Richard I. (2009) Control of polymorphism in NaNbO3 by hydrothermal synthesis. Chemical Communications, Vol.45 (No.1). pp. 68-70. doi:10.1039/b814601b ISSN 1359-7345.
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Official URL: http://dx.doi.org/10.1039/b814601b
Abstract
The metastable ilmenite polymorph of NaNbO3, instead of the expected perovskite polymorph, may be prepared directly in one step under mild hydrothermal conditions by lowering pH and using close to stoichiometric amounts of metal precursors; in situ energy-dispersive X-ray diffraction shows that crystallisation occurs rapidly via a sequence of intermediate crystalline phases.
Item Type: | Journal Article | ||||
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Subjects: | Q Science > QD Chemistry | ||||
Divisions: | Faculty of Science, Engineering and Medicine > Science > Chemistry | ||||
Library of Congress Subject Headings (LCSH): | Polymorphism (Crystallography), Thermochemistry, Biosynthesis, Nuclear magnetic resonance, Crystallization, Oxides, Lead zirconate titanate, Sodium compounds | ||||
Journal or Publication Title: | Chemical Communications | ||||
Publisher: | Royal Society of Chemistry | ||||
ISSN: | 1359-7345 | ||||
Official Date: | 2009 | ||||
Dates: |
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Volume: | Vol.45 | ||||
Number: | No.1 | ||||
Number of Pages: | 3 | ||||
Page Range: | pp. 68-70 | ||||
DOI: | 10.1039/b814601b | ||||
Status: | Peer Reviewed | ||||
Publication Status: | Published | ||||
Access rights to Published version: | Restricted or Subscription Access | ||||
Funder: | Engineering and Physical Sciences Research Council (EPSRC) | ||||
Grant number: | EP/F012721/1 (EPSRC) |
Data sourced from Thomson Reuters' Web of Knowledge
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