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Estimation of internuclear couplings in the solid-state NMR of multiple-spin systems. Selective spin echoes and off-magic-angle sample spinning

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Pileio, Giuseppe, Mamone, S. (Salvatore), Mollica, Giulia, Montesinos, Ildefonso Marin, Gansmueller, Axel, Carravetta, Marina, Brown, Steven P. and Levitt, Malcolm H. (2008) Estimation of internuclear couplings in the solid-state NMR of multiple-spin systems. Selective spin echoes and off-magic-angle sample spinning. Chemical Physics Letters, Vol.456 (No.1-3). pp. 116-121. doi:10.1016/j.cplett.2008.03.021 ISSN 0009-2614.

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Official URL: http://dx.doi.org/10.1016/j.cplett.2008.03.021

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Abstract

Internuclear couplings between selected homonuclear spin pairs in a multiply-labelled spin system are determined by NMR spin echo experiments in the solid-state. The spin echoes are induced by an amplitude-modulated shaped pulse. The time shift in the echo modulation curve is treated by average Hamiltonian theory and verified by numerical simulation. The J-couplings may be estimated by experiments on samples spinning at the magic-angle, while the direct dipole-dipole couplings may be estimated by off-magic-angle spinning. The concept is tested on a uniformly C-13-enriched sample of L-histidine hydrochloride monohydrate. (C) 2008 Elsevier B.V. All rights reserved.

Item Type: Journal Article
Subjects: Q Science > QD Chemistry
Q Science > QC Physics
Divisions: Faculty of Science, Engineering and Medicine > Science > Physics
Library of Congress Subject Headings (LCSH): Nuclear magnetic resonance spectroscopy, Nuclear spin
Journal or Publication Title: Chemical Physics Letters
Publisher: Elsevier BV
ISSN: 0009-2614
Official Date: 21 April 2008
Dates:
DateEvent
21 April 2008Published
Volume: Vol.456
Number: No.1-3
Number of Pages: 6
Page Range: pp. 116-121
DOI: 10.1016/j.cplett.2008.03.021
Status: Peer Reviewed
Publication Status: Published
Access rights to Published version: Restricted or Subscription Access
Funder: Engineering and Physical Sciences Research Council (EPSRC)

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