Fox, David J., Parris, Sean, Pedersen, Daniel Sejer and Warren, Stuart (2008) (1R,2R)-4-Benzoyl-2-benzoyloxy-1-phenylbutyl imidazole-1-carboxylate. Acta Crystallographica. Section E: Structure Reports Online, Vol.64 (Part 3). O619-U1385. doi:10.1107/S1600536808004364 ISSN 1600-5368.

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Abstract

The title compound, C28H24N2O5, was prepared from (E)-2cinnamyl-1,3-diphenylpropane-1,3-dione using standard Sharpless asymmetric dihydroxylation conditions, followed by treatment with 1,1'-carbonyl diimidazole. In the crystal structure, the phenyl rings form intermolecular face-to-face pi-pi contacts, with an interplanar angle of 15.5 ( 2) and a centroid-centroid distance of 4.73 (1) angstrom. One phenyl ring also forms a C-H center dot center dot center dot pi contact to an adjacent imidazole ring, with an H center dot center dot center dot centroid distance of 3.18 angstrom.

Item Type:	Journal Article
Subjects:	Q Science > QD Chemistry
Divisions:	Faculty of Science, Engineering and Medicine > Science > Chemistry
Journal or Publication Title:	Acta Crystallographica. Section E: Structure Reports Online
Publisher:	Wiley-Blackwell Publishing, Inc.
ISSN:	1600-5368
Official Date:	March 2008
Dates:	Date Event March 2008 Published
Volume:	Vol.64
Number:	Part 3
Number of Pages:	12
Page Range:	O619-U1385
DOI:	10.1107/S1600536808004364
Status:	Peer Reviewed
Publication Status:	Published
Access rights to Published version:	Restricted or Subscription Access

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