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A high-resolution Ca-43 solid-state NMR study of the calcium sites of hydroxyapatite
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Laurencin, Danielle, Wong, Alan, Hanna, John V., Dupree, Ray and Smith, Mark E.. (2008) A high-resolution Ca-43 solid-state NMR study of the calcium sites of hydroxyapatite. Journal of the American Chemical Society, Vol.130 (No.8). pp. 2412-2413. ISSN 0002-7863
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Official URL: http://dx.doi.org/10.1021/ja710557t
Abstract
High resolution Ca-43 solid-state NMR studies of hydroxyapatite (Ca-10(PO4)(6)(OH2)) were performed at 14.1 T. The two crystallographically distinct calcium sites were unequivocally resolved by a triple-quantum magic angle spinning experiment, and the unambiguous assignment of the signals was possible using H-1-Ca-43 rotational echo double resonance and H-1-Ca-43 cross polarization magic angle spinning experiments.
| Item Type: | Journal Article |
|---|---|
| Subjects: | Q Science > QD Chemistry |
| Divisions: | Administration > Vice Chancellor's Office Faculty of Science > Physics |
| Journal or Publication Title: | Journal of the American Chemical Society |
| Publisher: | American Chemical Society |
| ISSN: | 0002-7863 |
| Date: | 27 February 2008 |
| Volume: | Vol.130 |
| Number: | No.8 |
| Number of Pages: | 2 |
| Page Range: | pp. 2412-2413 |
| Identification Number: | 10.1021/ja710557t |
| Status: | Peer Reviewed |
| Publication Status: | Published |
| Access rights to Published version: | Restricted or Subscription Access |
| URI: | http://wrap.warwick.ac.uk/id/eprint/30498 |
Data sourced from Thomson Reuters' Web of Knowledge
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