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Residual dipolar couplings by off-magic-angle spinning in solid-state nuclear magnetic resonance spectroscopy
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Pileio, Giuseppe, Guo, Ying, Pham, Tran N., Griffin, John M., Levitt, Malcolm H. and Brown, Steven P. (2007) Residual dipolar couplings by off-magic-angle spinning in solid-state nuclear magnetic resonance spectroscopy. Journal of the American Chemical Society, Vol.129 (No.36). pp. 10972-10973. doi:10.1021/ja0721115 ISSN 0002-7863.
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Official URL: http://dx.doi.org/10.1021/ja0721115
Abstract
A solid-state NMR analogue of the solution-state residual dipolar coupling effect is demonstrated. A small misset of the spinning axis by less than 0.5 degrees changes the modulation frequency of spin-echoes, allowing the estimation of internuclear dipole-dipole couplings and hence internuclear distances.
Item Type: | Journal Article | ||||
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Subjects: | Q Science > QD Chemistry | ||||
Divisions: | Faculty of Science, Engineering and Medicine > Science > Physics | ||||
Journal or Publication Title: | Journal of the American Chemical Society | ||||
Publisher: | American Chemical Society | ||||
ISSN: | 0002-7863 | ||||
Official Date: | 12 September 2007 | ||||
Dates: |
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Volume: | Vol.129 | ||||
Number: | No.36 | ||||
Number of Pages: | 2 | ||||
Page Range: | pp. 10972-10973 | ||||
DOI: | 10.1021/ja0721115 | ||||
Status: | Peer Reviewed | ||||
Publication Status: | Published | ||||
Access rights to Published version: | Restricted or Subscription Access |
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