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A Al-27 MAS NMR study of a sol-gel produced alumina: Identification of the NMR parameters of the theta-Al2O3 transition alumina phase
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O'Dell, L. A., Savin, S. L. P., Chadwick, A. V. and Smith, Mark E. (2007) A Al-27 MAS NMR study of a sol-gel produced alumina: Identification of the NMR parameters of the theta-Al2O3 transition alumina phase. Solid State Nuclear Magnetic Resonance, Vol.31 (No.4). pp. 169-173. doi:10.1016/j.ssnmr.2007.05.002 ISSN 0926-2040.
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Official URL: http://dx.doi.org/10.1016/j.ssnmr.2007.05.002
Abstract
Al-27 MAS NMR has been used to study a sol-gel prepared alumina annealed at various temperatures. Two-field simulation of the sample heated to 1200 degrees C confirmed the presence of corundum, as suggested by XRD, and also the presence of nanocrystalline theta-Al2O3. Al-27 MAS NMR chemical shifts, quadrupolar coupling constants and asymmetry parameters are reported for the tetrahedral and octahedral aluminium sites within theta-Al2O3.
Item Type: | Journal Article | ||||
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Subjects: | Q Science > QD Chemistry Q Science > QC Physics |
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Divisions: | Administration > University Executive Office Faculty of Science, Engineering and Medicine > Science > Physics |
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Journal or Publication Title: | Solid State Nuclear Magnetic Resonance | ||||
Publisher: | Academic Press | ||||
ISSN: | 0926-2040 | ||||
Official Date: | July 2007 | ||||
Dates: |
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Volume: | Vol.31 | ||||
Number: | No.4 | ||||
Number of Pages: | 5 | ||||
Page Range: | pp. 169-173 | ||||
DOI: | 10.1016/j.ssnmr.2007.05.002 | ||||
Status: | Peer Reviewed | ||||
Publication Status: | Published | ||||
Access rights to Published version: | Restricted or Subscription Access |
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