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Characterisation of nanocrystalline magnesium oxide by X-ray absorption spectroscopy
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Savin, Shelley L. P., Chadwick, Alan V., O'Dell, Luke A. and Smith, Mark E. (2007) Characterisation of nanocrystalline magnesium oxide by X-ray absorption spectroscopy. ChemPhysChem, Vol.8 (No.6). pp. 882-889. doi:10.1002/cphc.200600750 ISSN 1439-4235.
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Official URL: http://dx.doi.org/10.1002/cphc.200600750
Abstract
27Al MAS NMR has been used to study a sol–gel prepared alumina annealed at various temperatures. Two-field simulation of the sample heated to 1200 °C confirmed the presence of corundum, as suggested by XRD, and also the presence of nanocrystalline θ-Al2O3. 27Al MAS NMR chemical shifts, quadrupolar coupling constants and asymmetry parameters are reported for the tetrahedral and octahedral aluminium sites within θ-Al2O3.
Item Type: | Journal Article | ||||
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Subjects: | Q Science > QD Chemistry Q Science > QC Physics |
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Divisions: | Administration > University Executive Office Faculty of Science, Engineering and Medicine > Science > Physics |
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Journal or Publication Title: | ChemPhysChem | ||||
Publisher: | Wiley - V C H Verlag GmbH & Co. KGaA | ||||
ISSN: | 1439-4235 | ||||
Official Date: | 23 April 2007 | ||||
Dates: |
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Volume: | Vol.8 | ||||
Number: | No.6 | ||||
Number of Pages: | 8 | ||||
Page Range: | pp. 882-889 | ||||
DOI: | 10.1002/cphc.200600750 | ||||
Status: | Peer Reviewed | ||||
Publication Status: | Published | ||||
Access rights to Published version: | Restricted or Subscription Access |
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