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A solid-state O-17 NMR study of local order and crystallinity in amine-templated mesoporous Nb oxide
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Skadtchenko, Boris O., Rao, Yuxiang, Kemp, Thomas F., Bhattacharya, Prodipta, Thomas, Pam A., Trudeau, Michel, Smith, Mark E. and Antonelli, Dave M. (2007) A solid-state O-17 NMR study of local order and crystallinity in amine-templated mesoporous Nb oxide. Angewandte Chemie (International Edition), Volume 46 (Number 15). pp. 2635-2638. doi:10.1002/anie.200604602 ISSN 1433-7851.
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Official URL: http://dx.doi.org/10.1002/anie.200604602
Abstract
Order locally: 17O magic-angle-spinning NMR spectroscopy of bulk sol–gel-prepared Nb2O5 and mesoporous, template-free Nb2O5 (see picture) shows very high local order in the mesoporous sample. The oxygen atoms are coordinated only as ONb2 in contrast with bulk phases in which the oxygen atoms are always present in a mixture of ONb2 and ONb3 coordination environments.
Item Type: | Journal Article | ||||
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Subjects: | Q Science > QD Chemistry | ||||
Divisions: | Faculty of Science, Engineering and Medicine > Science > Physics | ||||
Journal or Publication Title: | Angewandte Chemie (International Edition) | ||||
Publisher: | Wiley - V C H Verlag GmbH & Co. KGaA | ||||
ISSN: | 1433-7851 | ||||
Official Date: | 2007 | ||||
Dates: |
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Volume: | Volume 46 | ||||
Number: | Number 15 | ||||
Number of Pages: | 4 | ||||
Page Range: | pp. 2635-2638 | ||||
DOI: | 10.1002/anie.200604602 | ||||
Status: | Peer Reviewed | ||||
Publication Status: | Published |
Data sourced from Thomson Reuters' Web of Knowledge
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