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High-resolution and sensitivity through-bond correlations in ultra-fast magic angle spinning (MAS) solid-state NMR
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Bertini, Ivano, Emsley, Lyndon, Felli, Isabella C., Laage, Ségolène, Lesage, Anne, Lewandowski, Józef R., Marchetti, A. (Alessandro), Pierattelli, Roberta and Pintacuda, Guido (2011) High-resolution and sensitivity through-bond correlations in ultra-fast magic angle spinning (MAS) solid-state NMR. Chemical Science, Vol.2 (No.2). pp. 345-348. doi:10.1039/c0sc00397b ISSN 2041-6520.
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Official URL: http://dx.doi.org/10.1039/c0sc00397b
Abstract
We introduce a new experiment, which makes use of Spin State Selective manipulations to perform sensitive and resolved through-bond correlations in organic and biological solids at high-fields and under ultra-fast MAS. The scheme is the shortest and most sensitive through-bond correlation method introduced so far in solids, yields resolved fingerprints of uniformly (13)C-labeled biomolecules, and constitutes a tool to highlight slight static structural disorder around crystallographically equivalent molecules in microcrystalline samples.
| Item Type: | Journal Article | ||||
|---|---|---|---|---|---|
| Subjects: | Q Science > QD Chemistry | ||||
| Divisions: | Faculty of Science, Engineering and Medicine > Science > Chemistry | ||||
| Library of Congress Subject Headings (LCSH): | Nuclear magnetic resonance spectroscopy, Solid state chemistry | ||||
| Journal or Publication Title: | Chemical Science | ||||
| Publisher: | Royal Society of Chemistry | ||||
| ISSN: | 2041-6520 | ||||
| Official Date: | 1 February 2011 | ||||
| Dates: |
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| Volume: | Vol.2 | ||||
| Number: | No.2 | ||||
| Page Range: | pp. 345-348 | ||||
| DOI: | 10.1039/c0sc00397b | ||||
| Status: | Peer Reviewed | ||||
| Publication Status: | Published | ||||
| Access rights to Published version: | Restricted or Subscription Access | ||||
| Funder: | France. Agence nationale de la recherche (ANR), Ente Cassa di risparmio di Firenze, Universita Italo Francese, Sixth Framework Programme (European Commission) (FP6), European Union (EU) | ||||
| Grant number: | ANR 08-BLAN-0035-01 (ANR), 22397RJ (ECRF), RII3-026145 (FP6), PIRG03-GA-2008-231026 (EU) |
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