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High-resolution and sensitivity through-bond correlations in ultra-fast magic angle spinning (MAS) solid-state NMR

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Bertini, Ivano, Emsley, Lyndon, Felli, Isabella C., Laage, Ségolène, Lesage, Anne, Lewandowski, Józef R., Marchetti, A. (Alessandro), Pierattelli, Roberta and Pintacuda, Guido (2011) High-resolution and sensitivity through-bond correlations in ultra-fast magic angle spinning (MAS) solid-state NMR. Chemical Science, Vol.2 (No.2). pp. 345-348. doi:10.1039/c0sc00397b ISSN 2041-6520.

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Official URL: http://dx.doi.org/10.1039/c0sc00397b

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Abstract

We introduce a new experiment, which makes use of Spin State Selective manipulations to perform sensitive and resolved through-bond correlations in organic and biological solids at high-fields and under ultra-fast MAS. The scheme is the shortest and most sensitive through-bond correlation method introduced so far in solids, yields resolved fingerprints of uniformly (13)C-labeled biomolecules, and constitutes a tool to highlight slight static structural disorder around crystallographically equivalent molecules in microcrystalline samples.

Item Type: Journal Article
Subjects: Q Science > QD Chemistry
Divisions: Faculty of Science, Engineering and Medicine > Science > Chemistry
Library of Congress Subject Headings (LCSH): Nuclear magnetic resonance spectroscopy, Solid state chemistry
Journal or Publication Title: Chemical Science
Publisher: Royal Society of Chemistry
ISSN: 2041-6520
Official Date: 1 February 2011
Dates:
DateEvent
1 February 2011Published
Volume: Vol.2
Number: No.2
Page Range: pp. 345-348
DOI: 10.1039/c0sc00397b
Status: Peer Reviewed
Publication Status: Published
Access rights to Published version: Restricted or Subscription Access
Funder: France. Agence nationale de la recherche (ANR), Ente Cassa di risparmio di Firenze, Universita Italo Francese, Sixth Framework Programme (European Commission) (FP6), European Union (EU)
Grant number: ANR 08-BLAN-0035-01 (ANR), 22397RJ (ECRF), RII3-026145 (FP6), PIRG03-GA-2008-231026 (EU)

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