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Coupling of Heck and hydrogenation reactions in a continuous compact reactor
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Fan, Xiaolei, Plucinski, Pawel K. and Lapkin, Alexei (2009) Coupling of Heck and hydrogenation reactions in a continuous compact reactor. In: The 8th World Congress of Chemical Engineering (WCCE8), Montreal, Quebec, Canada, Aug 23-27, 2009 doi:10.1016/j.jcat.2009.07.019
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Official URL: http://www.wcce8.org/techsched/00001321.htm
Abstract
Synthesis of dibenzene via sequential Heck C-C coupling and alkene hydrogenation reactions catalysed by Pd/C was demonstrated using an intensified multifunctional flow reactor. Sequential addition of inert gas and hydrogen was found to be essential to avoid side products formation in the Heck section of the reactor. Reverse flow operation was shown to be effective for retaining the leached Pd from the Heck section of the reactor.
Item Type: | Conference Item (Speech) | ||||
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Subjects: | T Technology > TA Engineering (General). Civil engineering (General) T Technology > TP Chemical technology |
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Divisions: | Faculty of Science, Engineering and Medicine > Engineering > Engineering | ||||
Official Date: | 2009 | ||||
Dates: |
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DOI: | 10.1016/j.jcat.2009.07.019 | ||||
Status: | Not Peer Reviewed | ||||
Publication Status: | Published | ||||
Funder: | Engineering and Physical Sciences Research Council (EPSRC) | ||||
Grant number: | EP/C519736/1 | ||||
Conference Paper Type: | Speech | ||||
Title of Event: | The 8th World Congress of Chemical Engineering (WCCE8) | ||||
Type of Event: | Other | ||||
Location of Event: | Montreal, Quebec, Canada | ||||
Date(s) of Event: | Aug 23-27, 2009 |
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