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Dynamic HPLC study of C-70 chlorination reveals a surprisingly selective synthesis of C70Cl8
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Kuvychko, Igor V., Popov, Alexey A., Streletskii, Alexey V., Nye, Leanne C., Drewello, Thomas, Strauss, Steven H. and Boltalina, Olga V. (2010) Dynamic HPLC study of C-70 chlorination reveals a surprisingly selective synthesis of C70Cl8. Chemical Communications, Vol.46 (No.43). pp. 8204-8206. doi:10.1039/c0cc03134h
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Official URL: http://dx.doi.org/10.1039/c0cc03134h
Abstract
A dynamic HPLC study of C-70 chlorination led to the discovery, isolation, characterization, and development of the efficient preparatory procedures for two previously unknown soluble chlorofullerenes C70Cl8 and C70Cl6 and for insoluble [C70Cl8](n). A novel synthesis of 99% pure C70Cl10 with a nearly quantitative yield was also developed. The first stability study of C70Cl10,8,6 in solution showed that these compounds are very light-sensitive.
| Item Type: | Journal Article | ||||
|---|---|---|---|---|---|
| Subjects: | Q Science > QD Chemistry | ||||
| Divisions: | Faculty of Science > Chemistry | ||||
| Journal or Publication Title: | Chemical Communications | ||||
| Publisher: | Royal Society of Chemistry | ||||
| ISSN: | 1359-7345 | ||||
| Official Date: | 2010 | ||||
| Dates: |
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| Volume: | Vol.46 | ||||
| Number: | No.43 | ||||
| Number of Pages: | 3 | ||||
| Page Range: | pp. 8204-8206 | ||||
| DOI: | 10.1039/c0cc03134h | ||||
| Status: | Peer Reviewed | ||||
| Publication Status: | Published | ||||
| Access rights to Published version: | Restricted or Subscription Access | ||||
| Funder: | Alexander von Humboldt Foundation, U.S. NSF, Colorado State University Research Foundation | ||||
| Grant number: | CHE-0707223, CHE-1012468 |
Data sourced from Thomson Reuters' Web of Knowledge
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