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Dynamic HPLC study of C-70 chlorination reveals a surprisingly selective synthesis of C70Cl8

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Kuvychko, Igor V., Popov, Alexey A., Streletskii, Alexey V., Nye, Leanne C., Drewello, Thomas, Strauss, Steven H. and Boltalina, Olga V. (2010) Dynamic HPLC study of C-70 chlorination reveals a surprisingly selective synthesis of C70Cl8. Chemical Communications, Vol.46 (No.43). pp. 8204-8206. doi:10.1039/c0cc03134h

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Official URL: http://dx.doi.org/10.1039/c0cc03134h

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Abstract

A dynamic HPLC study of C-70 chlorination led to the discovery, isolation, characterization, and development of the efficient preparatory procedures for two previously unknown soluble chlorofullerenes C70Cl8 and C70Cl6 and for insoluble [C70Cl8](n). A novel synthesis of 99% pure C70Cl10 with a nearly quantitative yield was also developed. The first stability study of C70Cl10,8,6 in solution showed that these compounds are very light-sensitive.

Item Type: Journal Article
Subjects: Q Science > QD Chemistry
Divisions: Faculty of Science > Chemistry
Journal or Publication Title: Chemical Communications
Publisher: Royal Society of Chemistry
ISSN: 1359-7345
Official Date: 2010
Dates:
DateEvent
2010Published
Volume: Vol.46
Number: No.43
Number of Pages: 3
Page Range: pp. 8204-8206
DOI: 10.1039/c0cc03134h
Status: Peer Reviewed
Publication Status: Published
Access rights to Published version: Restricted or Subscription Access
Funder: Alexander von Humboldt Foundation, U.S. NSF, Colorado State University Research Foundation
Grant number: CHE-0707223, CHE-1012468

Data sourced from Thomson Reuters' Web of Knowledge

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