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High hydrostatic pressure equipment for neutron scattering studies of samples in solutions
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Peters, Judith, Trapp, Marcus, Hughes, Darren J., Rowe, Steven, Demé, Bruno, Laborier, Jean-Luc, Payre, Claude, Gonzales, Jean-Paul, Baudoin, Simon, Belkhier, Nadir and Lelièvre-Berna, Eddy (2012) High hydrostatic pressure equipment for neutron scattering studies of samples in solutions. High Pressure Research, Vol.32 (No.1). pp. 97-102. doi:10.1080/08957959.2011.642376 ISSN 0895-7959.
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Official URL: http://dx.doi.org/10.1080/08957959.2011.642376
Abstract
The design of new high pressure equipment for structural and dynamical studies on samples in solution is described. We present two sample cells for applying pressures up to 150 and 700 MPa (i.e. 1.5 and 7 kbar), respectively. These cells are mounted on special sticks and inserted into the calorimeter of a cryostat to regulate the temperature. Different parts of the equipment – the pressure controller, the sticks and the cells – are described. In addition, radiography tests which were performed with neutrons in situ at the Institut Laue Langevin to verify the tightness of the cells and the hydrostatic transmission of the pressure to the sample are presented. First results on model lipids are in agreement with former results by R. Winter et al. [Towards an understanding of the temperature/pressure configurational and free-energy landscape of biomolecules, J. Non-Equilib. Thermodyn. 32 (2007), pp. 41–97].
Item Type: | Journal Article | ||||
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Divisions: | Faculty of Science, Engineering and Medicine > Engineering > WMG (Formerly the Warwick Manufacturing Group) | ||||
Journal or Publication Title: | High Pressure Research | ||||
Publisher: | Taylor & Francis Inc. | ||||
ISSN: | 0895-7959 | ||||
Official Date: | 2012 | ||||
Dates: |
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Volume: | Vol.32 | ||||
Number: | No.1 | ||||
Page Range: | pp. 97-102 | ||||
DOI: | 10.1080/08957959.2011.642376 | ||||
Status: | Peer Reviewed | ||||
Publication Status: | Published | ||||
Access rights to Published version: | Restricted or Subscription Access |
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