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The dissolution mechanism of sulphur in hydrous silicate melts. I : assessment of analytical techniques in determining the sulphur speciation in iron-free to iron-poor glasses
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Klimm, Kevin, Kohn, Simon C., O'Dell, Luke A., Botcharnikov, Roman E. and Smith, Mark E. (2012) The dissolution mechanism of sulphur in hydrous silicate melts. I : assessment of analytical techniques in determining the sulphur speciation in iron-free to iron-poor glasses. Chemical Geology, Vol.322-323 . pp. 237-249. doi:10.1016/j.chemgeo.2012.04.027 ISSN 0009-2541.
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Official URL: http://dx.doi.org/10.1016/j.chemgeo.2012.04.027
Abstract
S K-edge XANES, λ (SKα) wavelength shift, 33S MAS NMR and Raman spectroscopy have been applied to a series of experimentally synthesised hydrous sulphur bearing silicate glasses to determine the oxidation state of sulphur dissolved in the glass. Glasses investigated include soda–lime glass (SLG), K2Si4O9 (KSG) and albitic (Albite) and trondhjemitic (TROND) glass compositions. The four spectroscopic techniques are compared with each other to investigate the applicability of each technique as a method to determine the sulphur oxidation state and structural aspects of sulphur dissolution in silicate melts.
Item Type: | Journal Article | ||||
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Divisions: | Faculty of Science, Engineering and Medicine > Science > Physics | ||||
Journal or Publication Title: | Chemical Geology | ||||
Publisher: | Elsevier BV | ||||
ISSN: | 0009-2541 | ||||
Official Date: | 2012 | ||||
Dates: |
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Volume: | Vol.322-323 | ||||
Page Range: | pp. 237-249 | ||||
DOI: | 10.1016/j.chemgeo.2012.04.027 | ||||
Status: | Peer Reviewed | ||||
Publication Status: | Published | ||||
Access rights to Published version: | Restricted or Subscription Access |
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