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Recent technique developments and applications of solid state NMR in characterising inorganic materials

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Hanna, John V. and Smith, Mark E.. (2010) Recent technique developments and applications of solid state NMR in characterising inorganic materials. Solid State Nuclear Magnetic Resonance, Vol.38 (No.1). pp. 1-18. ISSN 0926-2040

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Official URL: http://dx.doi.org/10.1016/j.ssnmr.2010.05.004

Abstract

A broad overview is given of some key recent developments in solid state NMR techniques that have driven enhanced applications to inorganic materials science. Reference is made to advances in hardware, pulse sequences and associated computational methods (e.g. first principles calculations, spectral simulation), along with their combination to provide more information about solid phases. The resulting methodology has allowed more nuclei to be observed and more structural information to be extracted. Cross referencing between experimental parameters and their calculation from the structure has given an added dimension to NMR as a characterisation probe of materials. Emphasis is placed on the progress made in the last decade especially from those nuclei that were little studied previously. The general points about technique development and the increased range of nuclei observed are illustrated through some specific exemplars from inorganic materials science.

Item Type:	Journal Article
Subjects:	Q Science > QD Chemistry Q Science > QC Physics
Divisions:	Administration > Vice Chancellor's Office Faculty of Science > Physics
Library of Congress Subject Headings (LCSH):	Nuclear magnetic resonance spectroscopy -- Methodology, Inorganic compounds
Journal or Publication Title:	Solid State Nuclear Magnetic Resonance
Publisher:	Academic Press
ISSN:	0926-2040
Official Date:	July 2010
Volume:	Vol.38
Number:	No.1
Number of Pages:	18
Page Range:	pp. 1-18
Identification Number:	10.1016/j.ssnmr.2010.05.004
Status:	Peer Reviewed
Publication Status:	Published
Access rights to Published version:	Restricted or Subscription Access
Funder:	Engineering and Physical Sciences Research Council (EPSRC), Higher Education Funding Council for England (HEFCE), University of Warwick, Advantage West Midlands (AWM), European Regional Development Fund (ERDF), Birmingham Science City
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URI:	http://wrap.warwick.ac.uk/id/eprint/5220