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Recent technique developments and applications of solid state NMR in characterising inorganic materials
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Hanna, John V. and Smith, Mark E. (2010) Recent technique developments and applications of solid state NMR in characterising inorganic materials. Solid State Nuclear Magnetic Resonance, Vol.38 (No.1). pp. 1-18. doi:10.1016/j.ssnmr.2010.05.004
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Official URL: http://dx.doi.org/10.1016/j.ssnmr.2010.05.004
Abstract
A broad overview is given of some key recent developments in solid state NMR techniques that have driven enhanced applications to inorganic materials science. Reference is made to advances in hardware, pulse sequences and associated computational methods (e.g. first principles calculations, spectral simulation), along with their combination to provide more information about solid phases. The resulting methodology has allowed more nuclei to be observed and more structural information to be extracted. Cross referencing between experimental parameters and their calculation from the structure has given an added dimension to NMR as a characterisation probe of materials. Emphasis is placed on the progress made in the last decade especially from those nuclei that were little studied previously. The general points about technique development and the increased range of nuclei observed are illustrated through some specific exemplars from inorganic materials science.
| Item Type: | Journal Article | ||||
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| Subjects: | Q Science > QD Chemistry Q Science > QC Physics |
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| Divisions: | Administration > University Executive Office Faculty of Science, Engineering and Medicine > Science > Physics |
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| Library of Congress Subject Headings (LCSH): | Nuclear magnetic resonance spectroscopy -- Methodology, Inorganic compounds | ||||
| Journal or Publication Title: | Solid State Nuclear Magnetic Resonance | ||||
| Publisher: | Academic Press | ||||
| ISSN: | 0926-2040 | ||||
| Official Date: | July 2010 | ||||
| Dates: |
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| Volume: | Vol.38 | ||||
| Number: | No.1 | ||||
| Number of Pages: | 18 | ||||
| Page Range: | pp. 1-18 | ||||
| DOI: | 10.1016/j.ssnmr.2010.05.004 | ||||
| Status: | Peer Reviewed | ||||
| Publication Status: | Published | ||||
| Access rights to Published version: | Restricted or Subscription Access | ||||
| Funder: | Engineering and Physical Sciences Research Council (EPSRC), Higher Education Funding Council for England (HEFCE), University of Warwick, Advantage West Midlands (AWM), European Regional Development Fund (ERDF), Birmingham Science City |
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