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Real-time synchrotron X-ray diffraction study on the isothermal martensite transformation of maraging steel in high magnetic fields

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San Martin, D., Jiménez-Melero, E., Duffy, J. A., Honkimäki, V., van der Zwaag, S. and van Dijk, N. H. (2012) Real-time synchrotron X-ray diffraction study on the isothermal martensite transformation of maraging steel in high magnetic fields. Journal of Applied Crystallography, Vol.45 (No.4). pp. 748-757. doi:10.1107/S0021889812024892 ISSN 0021-8898.

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Official URL: http://dx.doi.org/10.1107/S0021889812024892

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Abstract

The isothermal austenite-to-martensite transformation kinetics in a maraging steel have been studied by time-dependent microbeam diffraction measurements with high-energy X-rays. The transformation kinetics are shown to be accelerated significantly when a magnetic field of 8 T is applied. The average phase behaviour, obtained from a Rietveld refinement of the powder-averaged diffraction data, demonstrates that the martensite formation does not lead to a macroscopic strain in the austenite and martensite phases. An analysis of individual austenite reflections in the microbeam diffraction patterns, however, indicates that within the transforming austenite grains a transformation strain develops as a result of the formed martensite. The development of elastic strains during the transformation is explained by a partial strain confinement within the untransformed part of the austenite grain. The strain relaxation to the surrounding austenite grains is found to be dependent on the austenite volume. For a set of individual austenite grains the martensite nucleation is correlated with the initial austenite volume and the strain developed prior to the transformation as a result of martensite formation in the neighbouring grains.

Item Type: Journal Article
Divisions: Faculty of Science, Engineering and Medicine > Science > Physics
Journal or Publication Title: Journal of Applied Crystallography
Publisher: Wiley-Blackwell Publishing Ltd.
ISSN: 0021-8898
Official Date: 2012
Dates:
DateEvent
2012Published
Volume: Vol.45
Number: No.4
Page Range: pp. 748-757
DOI: 10.1107/S0021889812024892
Status: Peer Reviewed
Publication Status: Published
Access rights to Published version: Restricted or Subscription Access

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