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Organocatalytic, regioselective nucleophilic “click” addition of thiols to propiolic acid esters for polymer-polymer coupling
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Truong, Vinh X. and Dove, Andrew P. (2013) Organocatalytic, regioselective nucleophilic “click” addition of thiols to propiolic acid esters for polymer-polymer coupling. Angewandte Chemie International Edition, Volume 52 (Number 15). pp. 4132-4136. doi:10.1002/anie.201209239 ISSN 1433-7851.
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Official URL: http://dx.doi.org/10.1002/anie.201209239
Abstract
The regioselectivity of the nucleophilic addition of thiols to electron-deficient alkynes is controlled by the choice of the solvent (i.e. the polarity of the reaction mixture) and the catalyst. Both thioalkenes and dithianes can be prepared in a rapid reaction that generates no by-products (see scheme). In turn the utility of this reaction is shown for efficient end-group modification of polymers.
| Item Type: | Journal Article | ||||
|---|---|---|---|---|---|
| Divisions: | Faculty of Science, Engineering and Medicine > Science > Chemistry | ||||
| Journal or Publication Title: | Angewandte Chemie International Edition | ||||
| Publisher: | Wiley - V C H Verlag GmbH & Co. KGaA | ||||
| ISSN: | 1433-7851 | ||||
| Official Date: | 2013 | ||||
| Dates: |
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| Volume: | Volume 52 | ||||
| Number: | Number 15 | ||||
| Page Range: | pp. 4132-4136 | ||||
| DOI: | 10.1002/anie.201209239 | ||||
| Status: | Peer Reviewed | ||||
| Publication Status: | Published |
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