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Simultaneous acquisition of homonuclear and heteronuclear long-distance contacts with time-shared third spin assisted recoupling
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Lamley, Jonathan M. and Lewandowski, Józef R. (2012) Simultaneous acquisition of homonuclear and heteronuclear long-distance contacts with time-shared third spin assisted recoupling. Journal of Magnetic Resonance, Volume 218 . pp. 30-34. doi:10.1016/j.jmr.2012.03.013 ISSN 1090-7807.
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Official URL: http://dx.doi.org/10.1016/j.jmr.2012.03.013
Abstract
We present a time-shared Third Spin Assisted Recoupling (TSTSAR) experiment that allows for simultaneous acquisition of homonuclear (13C–13C) and heteronuclear (15N–13C) long-distance contacts in biomolecular solids under magic angle spinning. TSTSAR leads to substantial time savings and increases the information content of 2D correlation spectra.
| Item Type: | Journal Article | ||||
|---|---|---|---|---|---|
| Divisions: | Faculty of Science, Engineering and Medicine > Science > Chemistry | ||||
| Journal or Publication Title: | Journal of Magnetic Resonance | ||||
| Publisher: | Academic Press | ||||
| ISSN: | 1090-7807 | ||||
| Official Date: | 2012 | ||||
| Dates: |
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| Volume: | Volume 218 | ||||
| Page Range: | pp. 30-34 | ||||
| DOI: | 10.1016/j.jmr.2012.03.013 | ||||
| Status: | Peer Reviewed | ||||
| Publication Status: | Published | ||||
| Access rights to Published version: | Restricted or Subscription Access |
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