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Iron/Tetramethylethylenediamine-catalyzed ambient-temperature coupling of alkyl grignard reagents and aryl chlorides
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Rushworth, Philip, Hulcoop, David G and Fox, David J. (2013) Iron/Tetramethylethylenediamine-catalyzed ambient-temperature coupling of alkyl grignard reagents and aryl chlorides. The Journal of Organic Chemistry, Volume 78 (Number 18). pp. 9517-9521. doi:10.1021/jo4016612
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Official URL: http://dx.doi.org/10.1021/jo4016612
Abstract
Tetramethylethylenediamine (TMEDA) acts as cheap and readily removed ligand in the iron-catalyzed coupling of alkyl Grignard reagents and activated aryl chlorides. The use of TMEDA allows for low ligand and iron catalyst loading as well as an increased reaction concentration and an ambient reaction temperature on a mole scale.
| Item Type: | Journal Article | ||||
|---|---|---|---|---|---|
| Divisions: | Faculty of Science > Chemistry | ||||
| Journal or Publication Title: | The Journal of Organic Chemistry | ||||
| Publisher: | American Chemical Society | ||||
| ISSN: | 0022-3263 | ||||
| Official Date: | 29 August 2013 | ||||
| Dates: |
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| Volume: | Volume 78 | ||||
| Number: | Number 18 | ||||
| Page Range: | pp. 9517-9521 | ||||
| DOI: | 10.1021/jo4016612 | ||||
| Status: | Peer Reviewed | ||||
| Publication Status: | Published | ||||
| Access rights to Published version: | Restricted or Subscription Access |
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