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Iron/Tetramethylethylenediamine-catalyzed ambient-temperature coupling of alkyl grignard reagents and aryl chlorides

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Rushworth, Philip, Hulcoop, David G and Fox, David J. (2013) Iron/Tetramethylethylenediamine-catalyzed ambient-temperature coupling of alkyl grignard reagents and aryl chlorides. The Journal of Organic Chemistry, Volume 78 (Number 18). pp. 9517-9521. doi:10.1021/jo4016612

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Official URL: http://dx.doi.org/10.1021/jo4016612

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Abstract

Tetramethylethylenediamine (TMEDA) acts as cheap and readily removed ligand in the iron-catalyzed coupling of alkyl Grignard reagents and activated aryl chlorides. The use of TMEDA allows for low ligand and iron catalyst loading as well as an increased reaction concentration and an ambient reaction temperature on a mole scale.

Item Type: Journal Article
Divisions: Faculty of Science > Chemistry
Journal or Publication Title: The Journal of Organic Chemistry
Publisher: American Chemical Society
ISSN: 0022-3263
Official Date: 29 August 2013
Dates:
DateEvent
29 August 2013Available
Volume: Volume 78
Number: Number 18
Page Range: pp. 9517-9521
DOI: 10.1021/jo4016612
Status: Peer Reviewed
Publication Status: Published
Access rights to Published version: Restricted or Subscription Access

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