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Time-lapse synchrotron X-ray diffraction to monitor conservation coatings for heritage lead in atmospheres polluted with oak-emitted volatile organic compounds
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Grayburn, Rosie, Dowsett, M. G., De Keersmaecker, Michel, Westenbrink, Eric W., Covington, James A., Crawford, James, Hand, M., Walker, David, Thomas, Pam A., Banerjee, Dipanjan and Adriaens, Annemie (2014) Time-lapse synchrotron X-ray diffraction to monitor conservation coatings for heritage lead in atmospheres polluted with oak-emitted volatile organic compounds. Corrosion Science, Volume 82 . pp. 280-289. doi:10.1016/j.corsci.2014.01.027
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Official URL: http://dx.doi.org/10.1016/j.corsci.2014.01.027
Abstract
We discuss the effectiveness of a lead tetradecanoate coating on lead to protect against harmful volatile organic compounds emitted from oak. The oak volatile organic compounds were characterized by GCMS and the major constituent was found to be acetic acid. Under the test conditions, the coating decreases the rate of corrosion by up to 75% compared to bare lead. The thickness of corrosion products on the sample was also calculated thus demonstrating the power of the time-lapse synchrotron radiation X-ray diffraction technique to deliver a quantitative estimate of the effectiveness of the coating.
| Item Type: | Journal Article | ||||||||||
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| Subjects: | Q Science > QC Physics Q Science > QD Chemistry Q Science > QP Physiology T Technology > TA Engineering (General). Civil engineering (General) T Technology > TD Environmental technology. Sanitary engineering |
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| Divisions: | Faculty of Science, Engineering and Medicine > Engineering > Engineering Faculty of Science, Engineering and Medicine > Science > Physics |
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| Library of Congress Subject Headings (LCSH): | Organic compounds -- Analysis, Corrosion and anti-corrosives, Volatile organic compounds , X-rays -- Diffraction , X-ray diffractometer | ||||||||||
| Journal or Publication Title: | Corrosion Science | ||||||||||
| Publisher: | Pergamon | ||||||||||
| ISSN: | 0010-938X | ||||||||||
| Official Date: | May 2014 | ||||||||||
| Dates: |
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| Volume: | Volume 82 | ||||||||||
| Page Range: | pp. 280-289 | ||||||||||
| DOI: | 10.1016/j.corsci.2014.01.027 | ||||||||||
| Status: | Peer Reviewed | ||||||||||
| Publication Status: | Published | ||||||||||
| Access rights to Published version: | Restricted or Subscription Access | ||||||||||
| Funder: | Franc Sever (ESRF Software Support), Eveeson Charitable Trust, BROAD US Foundation, Fonds Wetenschappelijk Onderzoek (FWO) |
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