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Time-lapse synchrotron X-ray diffraction to monitor conservation coatings for heritage lead in atmospheres polluted with oak-emitted volatile organic compounds

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Grayburn, Rosie, Dowsett, M. G., De Keersmaecker, Michel, Westenbrink, Eric W., Covington, James A., Crawford, James, Hand, M., Walker, David, Thomas, Pam A., Banerjee, Dipanjan and Adriaens, Annemie (2014) Time-lapse synchrotron X-ray diffraction to monitor conservation coatings for heritage lead in atmospheres polluted with oak-emitted volatile organic compounds. Corrosion Science, Volume 82 . pp. 280-289. doi:10.1016/j.corsci.2014.01.027

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Official URL: http://dx.doi.org/10.1016/j.corsci.2014.01.027

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Abstract

We discuss the effectiveness of a lead tetradecanoate coating on lead to protect against harmful volatile organic compounds emitted from oak. The oak volatile organic compounds were characterized by GCMS and the major constituent was found to be acetic acid. Under the test conditions, the coating decreases the rate of corrosion by up to 75% compared to bare lead. The thickness of corrosion products on the sample was also calculated thus demonstrating the power of the time-lapse synchrotron radiation X-ray diffraction technique to deliver a quantitative estimate of the effectiveness of the coating.

Item Type: Journal Article
Subjects: Q Science > QC Physics
Q Science > QD Chemistry
Q Science > QP Physiology
T Technology > TA Engineering (General). Civil engineering (General)
T Technology > TD Environmental technology. Sanitary engineering
Divisions: Faculty of Science, Engineering and Medicine > Engineering > Engineering
Faculty of Science, Engineering and Medicine > Science > Physics
Library of Congress Subject Headings (LCSH): Organic compounds -- Analysis, Corrosion and anti-corrosives, Volatile organic compounds , X-rays -- Diffraction , X-ray diffractometer
Journal or Publication Title: Corrosion Science
Publisher: Pergamon
ISSN: 0010-938X
Official Date: May 2014
Dates:
DateEvent
May 2014Published
3 February 2014Available
23 January 2014Accepted
27 November 2013Submitted
Volume: Volume 82
Page Range: pp. 280-289
DOI: 10.1016/j.corsci.2014.01.027
Status: Peer Reviewed
Publication Status: Published
Access rights to Published version: Restricted or Subscription Access
Funder: Franc Sever (ESRF Software Support), Eveeson Charitable Trust, BROAD US Foundation, Fonds Wetenschappelijk Onderzoek (FWO)

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