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The electrodeposition of silver from supercritical carbon dioxide/acetonitrile
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Bartlett, Philip N., Perdjon-Abel, Magdalena, Cook, David, Reid, Gillian, Levason, William, Cheng, Fei, Zhang, Wenjian, George, Michael W., Ke, Jie, Beanland, R. and Sloan, Jeremy (2013) The electrodeposition of silver from supercritical carbon dioxide/acetonitrile. ChemElectroChem, Volume 1 (Number 1). pp. 187-194. doi:10.1002/celc.201300131 ISSN 2196-0216.
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Official URL: http://dx.doi.org/10.1002/celc.201300131
Abstract
Cyclic voltammetry of silver coordination complexes in acetonitrile and in a single-phase supercritical carbon dioxide/acetonitrile (scCO2/CH3CN) system is reported. Five silver precursors are investigated: (1,5-cyclooctadiene)(hexafluoroacetylacetonato) silver(I) [Ag(hfac)(COD)], (hexafluoroacetylacetonato)(triphenylphosphine) silver(I) [Ag(hfac)(PPh3)], (perfluorooctanoato)bis(triphenylphosphine) silver(I) [Ag(CF3(CF2)6CO2)(PPh3)2], tetrakis(triphenylphosphine) silver(I) tetrafluoroborate [Ag(PPh3)4][BF4] and tetrakis(acetonitrile) silver(I) tetrafluoroborate [Ag(CH3CN)4][BF4]. Of these, [Ag(CH3CN)4][BF4] is found to be the most suitable for electrodeposition of silver from scCO2/CH3CN.
| Item Type: | Journal Article | ||||
|---|---|---|---|---|---|
| Divisions: | Faculty of Science, Engineering and Medicine > Science > Physics | ||||
| Journal or Publication Title: | ChemElectroChem | ||||
| Publisher: | Wiley - V C H Verlag GmbH & Co. KGaA | ||||
| ISSN: | 2196-0216 | ||||
| Official Date: | 3 January 2013 | ||||
| Dates: |
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| Volume: | Volume 1 | ||||
| Number: | Number 1 | ||||
| Page Range: | pp. 187-194 | ||||
| DOI: | 10.1002/celc.201300131 | ||||
| Status: | Peer Reviewed | ||||
| Publication Status: | Published | ||||
| Access rights to Published version: | Open Access (Creative Commons) |
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