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Thermogravimetry and insitu mass spectrometry at high temperatures compared to thermochemical modelling – the weight loss during selective decarburisation at 800°C

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Auinger, Michael, Vogel, A., Praig, V. G., Danninger, H. and Rohwerder, Michael (2013) Thermogravimetry and insitu mass spectrometry at high temperatures compared to thermochemical modelling – the weight loss during selective decarburisation at 800°C. Corrosion Science, Volume 78 . pp. 188-192. doi:10.1016/j.corsci.2013.09.015 ISSN 0010-938X.

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Official URL: http://dx.doi.org/10.1016/j.corsci.2013.09.015

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Abstract

The insitu mass spectrometry detection of volatile species during high temperature corrosion processes,
exemplified by decarburisation of plain carbon steel, will be presented. Without influencing the thermobalance
signal, changes of the gas composition can be measured by introducing a small quartz capillary
into the reaction chamber in close proximity to the sample surface.
Experiments with the eutectoid composition Fe, 0.8 wt% C have been chosen intentionally as this alloy
represents one of the most intensely studied compositions in steel research. This allows good verification
with commonly accepted knowledge. Furthermore, comparison between experimental observations and
theoretical simulations will be given and critically discussed.

Item Type: Journal Article
Divisions: Faculty of Science, Engineering and Medicine > Engineering > WMG (Formerly the Warwick Manufacturing Group)
Journal or Publication Title: Corrosion Science
Publisher: Pergamon
ISSN: 0010-938X
Official Date: 12 October 2013
Dates:
DateEvent
12 October 2013Published
29 September 2013Accepted
3 April 2013Published
Volume: Volume 78
Page Range: pp. 188-192
DOI: 10.1016/j.corsci.2013.09.015
Status: Peer Reviewed
Publication Status: Published
Access rights to Published version: Restricted or Subscription Access

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