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Synthesis and NMR characterization of titanium and zirconium oxides incorporated in SBA-15
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Degirmenci, Volkan, Erdem, Özlen Ferruh, Ergun, Orcun, Yilmaz, Aysen, Michel, Dieter and Uner, Deniz (2008) Synthesis and NMR characterization of titanium and zirconium oxides incorporated in SBA-15. Topics in Catalysis, Volume 49 (Number 3-4). pp. 204-208. doi:10.1007/s11244-008-9078-z ISSN 1022-5528.
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Official URL: http://dx.doi.org/10.1007/s11244-008-9078-z
Abstract
Single oxides of Ti and Zr incorporated SBA-15 were prepared and characterized by N2 adsorption, NMR, and XPS techniques. 29Si MAS NMR results suggest the formation of Si–O–X linkages (X: Ti or Zr) by an increase in the ratio of Q 3/Q 4 in the presence of Ti or Zr. XPS analysis of Ti–SBA-15 catalysts indicate the presence of Ti–O–Si bonds in addition to Ti–O–Ti and Si–O–Si bonds, supporting the NMR evidence.
Item Type: | Journal Article | ||||
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Divisions: | Faculty of Science, Engineering and Medicine > Engineering > Engineering | ||||
Journal or Publication Title: | Topics in Catalysis | ||||
Publisher: | Springer New York LLC | ||||
ISSN: | 1022-5528 | ||||
Official Date: | August 2008 | ||||
Dates: |
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Volume: | Volume 49 | ||||
Number: | Number 3-4 | ||||
Page Range: | pp. 204-208 | ||||
DOI: | 10.1007/s11244-008-9078-z | ||||
Status: | Peer Reviewed | ||||
Publication Status: | Published | ||||
Access rights to Published version: | Restricted or Subscription Access |
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