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Tethered Ru(II) catalysts containing a Ru–I bond

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Jolley, Katherine E., Clarkson, Guy J. and Wills, Martin (2015) Tethered Ru(II) catalysts containing a Ru–I bond. Journal of Organometallic Chemistry, 776 . pp. 157-162. doi:10.1016/j.jorganchem.2014.10.033 ISSN 0022-328X.

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Official URL: http://dx.doi.org/10.1016/j.jorganchem.2014.10.033

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Abstract

Two new iodide-containing derivatives of the widely-adopted arene/Ru(II)/TsDPEN catalysts have been prepared and fully characterised, including through X-ray crystallography. They have been evaluated as catalysts for the asymmetric reduction of acetophenone under both transfer (ATH) and pressure hydrogenation (AH) conditions. The iodide-containing complexes are equally efficient in the ATH reaction, but less active in the AH reaction compared to the chloride derivatives.

Item Type: Journal Article
Subjects: Q Science > QD Chemistry
Divisions: Faculty of Science, Engineering and Medicine > Science > Chemistry
Library of Congress Subject Headings (LCSH): Ruthenium catalysts
Journal or Publication Title: Journal of Organometallic Chemistry
Publisher: Elsevier S.A.
ISSN: 0022-328X
Official Date: 14 January 2015
Dates:
DateEvent
14 January 2015Published
5 November 2014Available
23 October 2014Accepted
5 August 2014Submitted
Volume: 776
Number of Pages: 6
Page Range: pp. 157-162
DOI: 10.1016/j.jorganchem.2014.10.033
Status: Peer Reviewed
Publication Status: Published
Access rights to Published version: Restricted or Subscription Access
Date of first compliant deposit: 31 December 2015
Date of first compliant Open Access: 31 December 2015
Funder: Engineering and Physical Sciences Research Council (EPSRC), Birmingham Science City, Advantage West Midlands (AWM), European Regional Development Fund (ERDF)

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