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Data for Total synthesis of the Azolemycins
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Fox, David J. (2015) Data for Total synthesis of the Azolemycins. [Dataset]
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Official URL: http://wrap.warwick.ac.uk/74514
Abstract
The first total syntheses of newly isolated polyazole natural products azolemycins A–D, along with the synthesis of the tetra-oxazole non-natural analogue, are described.
Item Type: | Dataset | ||||||
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Subjects: | Q Science > QD Chemistry | ||||||
Divisions: | Faculty of Science, Engineering and Medicine > Science > Chemistry | ||||||
Type of Data: | Chemical synthesis, compounds | ||||||
Library of Congress Subject Headings (LCSH): | Organic compounds -- Synthesis | ||||||
Publisher: | University of Warwick, Department of Chemistry | ||||||
Official Date: | 17 December 2015 | ||||||
Dates: |
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Status: | Not Peer Reviewed | ||||||
Publication Status: | Published | ||||||
Media of Output (format): | .pdf .txt .par .doc | ||||||
Access rights to Published version: | Open Access (Creative Commons) | ||||||
Description: | Total Synthesis of Azolemycin A and Related Compounds, 1) Experimental details, Numbering system, N-tert-Butyloxycarbonyl-L-valine 7, N-tert-Butoxy-L-serine 9, (S)-3-(tert-Butoxycarbonyl)-2,2-dimethyloxazolidine-4-carboxylic acid 10, Dipeptide 11, Oxazole Methyl Ester 5 and Alkene 13, Asymmetric Dihydroxylation of Alkene 13, Preparation of activated MnO2, Tripeptide Oxazole 14, Bisoxazole 4, Preparation of Model Isoleucine Oxazoles, N-tertButoxycarbonyl-L-isoleucine, N-tertButoxycarbonyl-L-isoleucine and N-tertButoxycarbonyl-D-allo-isoleucine, N-tertButoxycarbonyl-L-isoleucyl-L-serine methyl ester, N-tertButoxycarbonyl-L-isoleucyl- and N-tertButoxycarbonyl-D-allo-isoleucyl-L-serine methyl ester, (2S, 3S) Isoleucine Oxazole, (2S, 3S) and (2R, 3S) Oxazole, Bisoxazole Acid, Pentapeptide 15, Pentapeptide Silyl Ether 16, Thioamide Silyl Ether 17, Thioamide 18, Thiazole 19, Tetrazole Carboxylic Acid 20, Hexapeptide 21, Hexapeptide hydrochloride, (S)-2-Hydroxy-3-methylbutanoic acid 22, Heptapeptide 23, Ketone 24, Azolemycin A 1a and Azolemycin B 1b, Azolemycin C 2a and Azolemycin D 2b, Tetraoxazole Methyl Ester 25, Tetraoxazole Carboxylic Acid 26, Tetraoxazole Hexapeptide 27, Tetraoxazole Alcohol 28, Tetraoxazole Ketone 29, Tetraoxazole Analogue 30, 2) References |
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Date of first compliant deposit: | 22 December 2015 | ||||||
RIOXX Funder/Project Grant: |
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