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Optically generated hyperpolarization for sensitivity enhancement in solution-state NMR spectroscopy

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Dale, Matthew W. and Wedge, Christopher (2016) Optically generated hyperpolarization for sensitivity enhancement in solution-state NMR spectroscopy. Chemical Communications, 52 (90). pp. 13221-13224. doi:10.1039/C6CC06651H

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Official URL: http://dx.doi.org/10.1039/C6CC06651H

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Abstract

We show that optical excitation of radical triplet pair systems can produce a fourfold NMR signal enhancement in solution, without the need for microwave pumping. Development of optical hyperpolarization methods will significantly impact all NMR user groups by boosting sensitivity and reducing signal averaging times.

Item Type: Journal Article
Subjects: Q Science > QD Chemistry
T Technology > TA Engineering (General). Civil engineering (General)
Divisions: Faculty of Science, Engineering and Medicine > Science > Physics
Library of Congress Subject Headings (LCSH): Nuclear magnetic resonance spectroscopy, Chemistry, Biochemistry , Materials science
Journal or Publication Title: Chemical Communications
Publisher: Royal Society of Chemistry
ISSN: 1359-7345
Official Date: 21 November 2016
Dates:
DateEvent
30 September 2016Available
21 November 2016Published
30 September 2016Accepted
12 August 2016Submitted
Volume: 52
Number: 90
Page Range: pp. 13221-13224
DOI: 10.1039/C6CC06651H
Status: Peer Reviewed
Publication Status: Published
Access rights to Published version: Restricted or Subscription Access
RIOXX Funder/Project Grant:
Project/Grant IDRIOXX Funder NameFunder ID
EP/N007875/1[EPSRC] Engineering and Physical Sciences Research Councilhttp://dx.doi.org/10.13039/501100000266
UNSPECIFIEDBruker Analytische Meßtechnik GmbHhttps://viaf.org/viaf/268533260
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