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Blocked isocyanates : from analytical and experimental considerations to non-polyurethane applications

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Rolph, Marianne S., Markowska, Anna L. J., Warriner, Colin N. and O'Reilly, Rachel K. (2016) Blocked isocyanates : from analytical and experimental considerations to non-polyurethane applications. Polymer Chemistry, 7 (48). pp. 7351-7364.

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Official URL: https://doi.org/10.1039%2Fc6py01776b

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Abstract

In this review we aim to provide an introductory guide to blocked isocyanates, through discussion on different examples of blocking groups, along with experimental considerations for their application. The review brings together updated examples of functionalities used and places specific emphasis on the analytical techniques used for the determination of deblocking temperature, updating previous reviews with the newly applied technique of X-ray photoelectron spectroscopy (XPS). Additionally, we put forward a brief update on the use of blocked isocyanates for other non-traditional polyurethane based polymer applications. We also highlight the importance of matching the analytical technique to the application of the blocked isocyanate, with differences in material state and experimental parameters having a great impact on the deblocking temperature reported.

Item Type: Journal Article
Subjects: T Technology > TP Chemical technology
Divisions: Faculty of Science > Chemistry
Library of Congress Subject Headings (LCSH): Isocyanates , Polyurethanes , X-ray photoelectron spectroscopy
Journal or Publication Title: Polymer Chemistry
Publisher: Royal Society of Chemistry
ISSN: 1759-9954
Official Date: 8 November 2016
Dates:
DateEvent
8 November 2016Published
7 November 2016Accepted
Volume: 7
Number: 48
Page Range: pp. 7351-7364
Status: Peer Reviewed
Publication Status: Published
Access rights to Published version: Open Access
Funder: Atomic Weapons Research Establishment (Great Britain), Engineering and Physical Sciences Research Council (EPSRC)

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